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Keras
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Hexane won’t mix with acetic acid, which is polar.
That’s why I’ll try DMSO. It’s polar, aprotic and has a boiling point well above that of Ac₂O.
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greenlight
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@paulll, yes, stoichiometrically the yields from phosphorus pentoxide reagent are terrible haha. I only need just over a 100 ml but even that's
probably pushing it.
@keras, are you sure glacial acetic acid isn't soluble in hexane? The SM wiki says it is and I'm sure I looked through a paper that said glacial
acetic acid is soluble all the way up to around octane the other day.
The only use for an atomic bomb is to keep somebody else from using one.
George Wald
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Keras
National Hazard
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Quote: Originally posted by greenlight  |
@keras, are you sure glacial acetic acid isn't soluble in hexane? The SM wiki says it is and I'm sure I looked through a paper that said glacial
acetic acid is soluble all the way up to around octane the other day.
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Well, best way is try it.  But I would be surprised!
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