Claisen flask

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The Claisen flask or Claisen distillation flask is a special type of distillation flask used in several procedures, like vacuum distillation. It was invented by Rainer Ludwig Claisen.

General

The Claisen flask is generally used for reduced-pressure distillation. The flask was designed to reduce the probability of having to repeat the distillation, due to bumping of the boiling liquid. It is similar to a Würtz flask, though the distinctive feature of the Claisen flask is a U-shaped neck fused on the top of the flask. The flask itself may be round-bottom or pear-shaped. The U-shape (or bifurcation) is similar to that of a Claisen adapter. This design makes it impossible for any splash of distilling liquid projected by bumping to reach the distillate.[1]

Some Claisen flasks have with a short fractionating column on the side arm.

Availability

Claisen flasks can be purchased from lab suppliers or online.

Projects

See also

References

  1. https://pubs.acs.org/doi/abs/10.1021/ed075p638
  2. http://www.sciencemadness.org/talk/viewthread.php?tid=16950

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