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Glyoxime, Diaminofurazan and Some Energetic Derivatives
Its preparation is in the DAAF patent I cited. Reduction of DAAF with AcOH-Zn then oxidation with ai ...
10-8-2008 at 12:13
by: Axt
Another caged nitramine
I wouldn't call it a caged structure, tricyclic.

I attached this previously, J. Org. Chem. vol. 5 ...
3-8-2008 at 12:12
by: Axt
5-nitro-3H-1,2,4-triazol-3-one (NTO)
Just different crystal forms, I really dont know if different polymorphs are being formed and which ...
26-7-2008 at 13:06
by: Axt
Metapurpurate
I wouldn't read too much into the "very sensitive to impact and friction", compared to what? TNT? I' ...
26-7-2008 at 12:46
by: Axt
5-nitro-3H-1,2,4-triazol-3-one (NTO)
I've prepared NTO via hydrazine + urea -> semicarbazide, glycerine + oxalic acid -> formic aci ...
26-7-2008 at 12:35
by: Axt
Metapurpurate
Theres another compound derived from picric acid (rather then the dinitro analogue) and presumably m ...
26-7-2008 at 01:54
by: Axt
3,4-Dicyanofuroxane (DCFO)
40°C melting point by itself is too low, performance 85% of TNT and a whole lot more expensive.

...
23-7-2008 at 12:16
by: Axt
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
"1 H-Tetrazolo[1,5-d]tetrazole: A solution of sodium nitrite (0.01 mol) in water (5 ml) was added dr ...
20-7-2008 at 23:31
by: Axt
Mellitic Acid Synthesis and Properties
Graphitic acid is explosive.

"Carbon from Graphitic Acid.-When graphitic acid is heated it explod ...
18-7-2008 at 23:19
by: Axt
Biguanide plus Biuret
I'm curious to know the use of the product? Its 8 membered melamine. The nitration product of melami ...
14-7-2008 at 23:39
by: Axt
Dissolving Bismuth, the road to Sodium Bismuthate, and other uses.
I had a try at sodium bismuthate. No real conclusions because I'm not real sure what this chocolate ...
14-7-2008 at 01:57
by: Axt
Hypergolic Reactions and Energetics
N2O4 detonates on mixing with N2H4. and rapidly ignites glyoxime.

To state the obvious Mn2O7 expl ...
10-7-2008 at 17:28
by: Axt
Halogenated Amines - the others
The tetrabrominated derivative of ethylenediamine was prepared. Its mentioned in the JCS article I a ...
10-7-2008 at 14:56
by: Axt
Halogenated Amines - the others
[quote][i]Originally posted by Axt[/i]
Another OTC possiblility is the dichloramine of isopropylami ...
10-7-2008 at 14:35
by: Axt
Glyoxime, Diaminofurazan and Some Energetic Derivatives
Arr your right, from the patent.

Dichloroglyoxime (HON:CClCCl:NOH), useful as an intermediate for ...
10-7-2008 at 12:20
by: Axt
Silver Nitrate + Ethanol = Ethyl Nitrate?
You failed to state you source of how you "know" this.

Checking scifinder yields your best bet wi ...
4-7-2008 at 13:16
by: Axt
Silver Nitrate + Ethanol = Ethyl Nitrate?
If you "know" something without doing it you must take it from a credible source (even then the word ...
4-7-2008 at 11:14
by: Axt
MEKP/Dynamite
Learn to type. If you dont care to make legible sentences, why should we care to read it let alone r ...
30-6-2008 at 12:04
by: Axt
Exotic Primaries - Complex Salts
Well, yes there is. However I don't see any reason to pop my eyes out over it.
22-6-2008 at 23:35
by: Axt
Electrophilic chlorination (no chlorine :-( )
I've posted the chlorination of benzene with TCCA, no (well, little) release of Cl2, very simple.

...
22-6-2008 at 23:20
by: Axt
Ammonium Perchlorate
Theres no such thing as "naclo3", "KCLO3", "NA2SO4" or "NACLO3". Go buy a text book (starting with E ...
20-6-2008 at 00:06
by: Axt
The Platinum Mirror
Patent US1935520 describes a copper-silver alloy mirror.

Patent Application IT19571029: A chem. C ...
16-6-2008 at 13:29
by: Axt
The Platinum Mirror
<b>A Method of Depositing Copper upon Glass from Aqueous Solutions in a Thin Brilliantly Refle ...
16-6-2008 at 13:14
by: Axt
Nitromethane HE purity required
72.2% NM
23.4% MeOH
4.4% Ethylenediamine

According to LLNL detonates at 5490m/s. I assume the c ...
14-6-2008 at 06:07
by: Axt
Preparation of cyanides
Thanks for the translation Schockwave, this may be the explanation for its explosive nature.

The ...
13-6-2008 at 11:12
by: Axt
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