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OTC tert-Butanol
[rquote=258794&tid=21341&author=Dave Angel][b]Wizzard[/b] (or anyone else for that matter) y ...
28-9-2012 at 16:10
by: Dave Angel
Birkeland-Eyde reactor for making nitric acid.
[rquote=256420&tid=1518&author=hissingnoise]An ozone generator with moisture-adjusted air fe ...
28-9-2012 at 16:02
by: Dave Angel
Acetic anhydride preparation
[rquote=260518&tid=9&author=Waffles SS]Interesting method[/rquote]
Interesting? I'd say rev ...
28-9-2012 at 09:35
by: Dave Angel
Tour My Lab
[rquote=260308&tid=4777&author=Pyro]
PS:who says chemistry and wine can't go together? :D[/ ...
25-9-2012 at 13:23
by: Dave Angel
Preparation of elemental phosphorus
Hey [b]Magpie[/b] - are you using something like this for your argon?:

[file]20343[/file]

I ma ...
25-9-2012 at 13:04
by: Dave Angel
Almost Tetralin...
This may be a long way round but it uses OTC/RA materials, of which I'm an advocate. The question is ...
25-9-2012 at 12:30
by: Dave Angel
Sodium!
Thanks both - your encouragement means a lot. 'Shoulders of giants' and all that though eh?

[rquo ...
25-9-2012 at 12:00
by: Dave Angel
Detritus
Similar musings were recently discussed in [url=http://www.sciencemadness.org/talk/viewthread.php?ti ...
23-9-2012 at 11:31
by: Dave Angel
Sodium!
[rquote=260053&tid=2103&author=BromicAcid]Love it Dave! My full scale Downs cell was a veri ...
23-9-2012 at 11:12
by: Dave Angel
Success!
I'm pleased to report that I've made sodium with my Castner cell :)

[b]Summary of recent work:[/b ...
22-9-2012 at 16:03
by: Dave Angel
Microwave nitrile synthesis from aldehydes
Another protential route to acetonitrile for exploration in this paper:

[file]20135[/file]

In ...
8-9-2012 at 16:02
by: Dave Angel
OTC tert-Butanol
[rquote=259242&tid=21341&author=jon]oh and just buy some mbte next time it's not hard to fin ...
8-9-2012 at 13:31
by: Dave Angel
Preparation of Tetralin?
Out of interest, is tetralin your specific goal or are you just looking for a reaction to do with th ...
8-9-2012 at 02:24
by: Dave Angel
Martin Fleischmann (1927 ─ 2012)
[rquote=259118&tid=21430&author=watson.fawkes]If you want some more wonder, take a look at t ...
8-9-2012 at 01:59
by: Dave Angel
Preparation of Tetralin?
I found a prep as part of a multi-step synthesis on Organic Syntheses:

http://www.orgsyn.org/orgs ...
6-9-2012 at 12:42
by: Dave Angel
What to do with tiny bits of Palladium wire?
Thanks for the trade offer [b]Fleaker[/b] but I think I'll hang onto them for now - I quite like the ...
6-9-2012 at 12:21
by: Dave Angel
Tungsten electrodes
1.6, 2.4 and 3.2 mm seem to be common diameters in the UK, with lengths of 150 mm, so in line with y ...
6-9-2012 at 11:56
by: Dave Angel
Martin Fleischmann (1927 ─ 2012)
[rquote=259062&tid=21430&author=unionised]All that from a failed experiment! Just imagine wh ...
6-9-2012 at 11:33
by: Dave Angel
Sodium!
[rquote=258392&tid=2103&author=m1tanker78]I started a thread but as I recall, it turned into ...
6-9-2012 at 11:24
by: Dave Angel
Martin Fleischmann (1927 ─ 2012)
I'd agree that his passing is not a 'great loss' to science as one might consider Feynmann and those ...
6-9-2012 at 10:53
by: Dave Angel
Martin Fleischmann (1927 ─ 2012)
[rquote=259037&tid=21430&author=hissingnoise][url=http://en.wikipedia.org/wiki/Martin_Fleisc ...
6-9-2012 at 09:55
by: Dave Angel
Tungsten electrodes
I stand enlightened; indeed they are green tipped, and I will be using these in my spot welder mk II ...
4-9-2012 at 12:48
by: Dave Angel
OTC tert-Butanol
Whilst HX may result in the tertiary haloalkane, it might be worth some experiments. I would not imm ...
3-9-2012 at 09:50
by: Dave Angel
Hook up a Vacuum cleaner to a Vacuum filtration system?
[rquote=258756&tid=21388&author=Endimion17]Put some kind of tubing through a cork that fits ...
3-9-2012 at 09:16
by: Dave Angel
Tungsten electrodes
[rquote=258009&tid=21234&author=elementcollector1]Would have to break a few lightbulbs, thou ...
1-9-2012 at 02:48
by: Dave Angel
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