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Making an Ozone Generator
For those who want to build an ozone generator with flyback, the oldest the tv is the better, in the ...
19-4-2015 at 07:25
by: Jimmymajesty
Silent discharge in preparative chemistry?
violet sin, thanks for the papers.

I tried out couple of things in the last days mainly with ace ...
19-4-2015 at 06:58
by: Jimmymajesty
Silent discharge in preparative chemistry?
Yup, I tried it out out today with Et-OH, but nothing really happened apart from after some time the ...
16-4-2015 at 12:12
by: Jimmymajesty
Using Quartz Glass Instead of Borosilicate Glass?
Hey Magpie,

That is the reason why I am turning graphite adapters to connect the quartz tube and ...
15-4-2015 at 09:08
by: Jimmymajesty
Silent discharge in preparative chemistry?
I finally had some time to try it out. I used 95% ethyl alcohol. Aluminum foil was wrapped around a ...
15-4-2015 at 08:58
by: Jimmymajesty
Silent discharge in preparative chemistry?
Hi,

I do not have references, the question is what woluld be the outcome if you refluxed simple c ...
13-4-2015 at 02:55
by: Jimmymajesty
Silent discharge in preparative chemistry?
Hi folks,

I am just wondering what useful chemicals could be made out of OTC chems with this meth ...
12-4-2015 at 14:06
by: Jimmymajesty
Oxidation of Isopropanol
That is indeed a nice graph, so how about...
1,oxidizing some copper as an anode with KNO3 electro ...
12-4-2015 at 10:22
by: Jimmymajesty
Making an Ozone Generator
I have just tried to use a homemade ozone generator to oxidize ethyl alcohol to acetic acid.

The ...
12-4-2015 at 09:35
by: Jimmymajesty
Using Quartz Glass Instead of Borosilicate Glass?
If you need some H2SO4 just go with Molecular Manipulations's route, dilute some nitric to 75% let S ...
11-4-2015 at 14:06
by: Jimmymajesty
Oxidation of Isopropanol
Hi byko3y

Try going with copper tube, or rather brass tube if you have it.
I do not think that i ...
11-4-2015 at 13:35
by: Jimmymajesty
toluene --> benzaldehyde
Thanks Magpie,
It was not actually a toaster but your guess was very close it was in some hotplate. ...
10-4-2015 at 13:37
by: Jimmymajesty
toluene --> benzaldehyde
Hi again,

Now that the weekend is coming and I am antisocial enough to spend the time in the gara ...
9-4-2015 at 11:49
by: Jimmymajesty
toluene --> benzaldehyde
I know it is slow and it is only a proof that it may be possible to make decent amount of bzaldehyde ...
8-4-2015 at 01:04
by: Jimmymajesty
toluene --> benzaldehyde
Hi Folks,

I did another 2 hrs run in the weekend but this time, -seeing Magpie's salicyl aldehyde ...
7-4-2015 at 12:47
by: Jimmymajesty
Nitromethane, nitroethane, nitropropane synthesis via industrial route
Hi Folks,

I did another microscale experiment.

The heating on the vial and reaction tube were ...
6-4-2015 at 22:13
by: Jimmymajesty
Phenyl cyanide or Benzonitrile synthesis
Thanks for the input but these chems are not OTC for me.
Its not the high temp I am worried about I ...
3-4-2015 at 23:31
by: Jimmymajesty
Phenyl cyanide or Benzonitrile synthesis
Hi again,

I gave some thought to it, so how about... dehydrating ethyl benzoate in the presence o ...
3-4-2015 at 11:42
by: Jimmymajesty
Nitromethane, nitroethane, nitropropane synthesis via industrial route
Praxichys you do not need to relieve the pressure after the reaction, you surely have to collect the ...
2-4-2015 at 09:08
by: Jimmymajesty
Nitromethane, nitroethane, nitropropane synthesis via industrial route
Magpie, like NurdRage says, we are here to explore the science:)
The 20kg PB tank is on its way, th ...
1-4-2015 at 09:12
by: Jimmymajesty
Preparation of Salicylaldehyde
Hey Magpie,

Well done!

I tried to isolate the acetaldehyde as the bisulhite adduct.
It needs ...
1-4-2015 at 08:59
by: Jimmymajesty
toluene --> benzaldehyde
IMHO it is not polite to ask someone why do you need this and that. I mean what is the point asking ...
1-4-2015 at 00:41
by: Jimmymajesty
Nitromethane, nitroethane, nitropropane synthesis via industrial route
so... I jerry-rigged a lil setup today.

I used a nebulizer to make HNO3 spray the entrainer was P ...
31-3-2015 at 12:50
by: Jimmymajesty
toluene --> benzaldehyde
Magpie, is hiring a glassblower really such big a deal? In every town there are at least two, they a ...
31-3-2015 at 12:29
by: Jimmymajesty
Nitromethane, nitroethane, nitropropane synthesis via industrial route
Hi folks,

I have been thinking how one could minimize the risk of explosion based on the run I di ...
29-3-2015 at 03:36
by: Jimmymajesty
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