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Nitromethane, nitroethane, nitropropane synthesis via industrial route
Hi there
I finally scavenged all the parts to my new gas phase reactor, which happens to be good ... |
23-10-2015 at 06:50
by: Jimmymajesty |
Acetic Acid Distillation with an Entrainer
Ethyl acetate can be used but it is really difficult to remove all the water with it from a 20% hous ... |
17-5-2015 at 12:25
by: Jimmymajesty |
Oxidation of Isopropanol
byko3y I thought you were after an efficient catalyst, if your goal is to get 10+ liters of acetone ... |
24-4-2015 at 00:47
by: Jimmymajesty |
Bad Habits In The Lab
I just find it odd or rather a paradox when I see a smoking chemist. All chemists especially we hobb ... |
23-4-2015 at 05:07
by: Jimmymajesty |
Bad Habits In The Lab
I always wondered why smoking chemists (hobbyist or professional) need protective equipments like fu ... |
22-4-2015 at 04:46
by: Jimmymajesty |
Oxidation of Isopropanol
I did a run today.
-the IPA was brought to boil, then the wattage on the kanthal wire was set so ... |
19-4-2015 at 11:03
by: Jimmymajesty |
Making an Ozone Generator
For those who want to build an ozone generator with flyback, the oldest the tv is the better, in the ... |
19-4-2015 at 07:25
by: Jimmymajesty |
Silent discharge in preparative chemistry?
violet sin, thanks for the papers.
I tried out couple of things in the last days mainly with ace ... |
19-4-2015 at 06:58
by: Jimmymajesty |
Silent discharge in preparative chemistry?
Yup, I tried it out out today with Et-OH, but nothing really happened apart from after some time the ... |
16-4-2015 at 12:12
by: Jimmymajesty |
Using Quartz Glass Instead of Borosilicate Glass?
Hey Magpie,
That is the reason why I am turning graphite adapters to connect the quartz tube and ... |
15-4-2015 at 09:08
by: Jimmymajesty |
Silent discharge in preparative chemistry?
I finally had some time to try it out. I used 95% ethyl alcohol. Aluminum foil was wrapped around a ... |
15-4-2015 at 08:58
by: Jimmymajesty |
Silent discharge in preparative chemistry?
Hi,
I do not have references, the question is what woluld be the outcome if you refluxed simple c ... |
13-4-2015 at 02:55
by: Jimmymajesty |
Silent discharge in preparative chemistry?
Hi folks,
I am just wondering what useful chemicals could be made out of OTC chems with this meth ... |
12-4-2015 at 14:06
by: Jimmymajesty |
Oxidation of Isopropanol
That is indeed a nice graph, so how about...
1,oxidizing some copper as an anode with KNO3 electro ... |
12-4-2015 at 10:22
by: Jimmymajesty |
Making an Ozone Generator
I have just tried to use a homemade ozone generator to oxidize ethyl alcohol to acetic acid.
The ... |
12-4-2015 at 09:35
by: Jimmymajesty |
Using Quartz Glass Instead of Borosilicate Glass?
If you need some H2SO4 just go with Molecular Manipulations's route, dilute some nitric to 75% let S ... |
11-4-2015 at 14:06
by: Jimmymajesty |
Oxidation of Isopropanol
Hi byko3y
Try going with copper tube, or rather brass tube if you have it.
I do not think that i ... |
11-4-2015 at 13:35
by: Jimmymajesty |
toluene --> benzaldehyde
Thanks Magpie,
It was not actually a toaster but your guess was very close it was in some hotplate. ... |
10-4-2015 at 13:37
by: Jimmymajesty |
toluene --> benzaldehyde
Hi again,
Now that the weekend is coming and I am antisocial enough to spend the time in the gara ... |
9-4-2015 at 11:49
by: Jimmymajesty |
toluene --> benzaldehyde
I know it is slow and it is only a proof that it may be possible to make decent amount of bzaldehyde ... |
8-4-2015 at 01:04
by: Jimmymajesty |
toluene --> benzaldehyde
Hi Folks,
I did another 2 hrs run in the weekend but this time, -seeing Magpie's salicyl aldehyde ... |
7-4-2015 at 12:47
by: Jimmymajesty |
Nitromethane, nitroethane, nitropropane synthesis via industrial route
Hi Folks,
I did another microscale experiment.
The heating on the vial and reaction tube were ... |
6-4-2015 at 22:13
by: Jimmymajesty |
Phenyl cyanide or Benzonitrile synthesis
Thanks for the input but these chems are not OTC for me.
Its not the high temp I am worried about I ... |
3-4-2015 at 23:31
by: Jimmymajesty |
Phenyl cyanide or Benzonitrile synthesis
Hi again,
I gave some thought to it, so how about... dehydrating ethyl benzoate in the presence o ... |
3-4-2015 at 11:42
by: Jimmymajesty |
Nitromethane, nitroethane, nitropropane synthesis via industrial route
Praxichys you do not need to relieve the pressure after the reaction, you surely have to collect the ... |
2-4-2015 at 09:08
by: Jimmymajesty |
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