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Amination of tertiary alkyl halide
Why do you keep saying tertiary alkyl halide? Isopropyl chloride is a secondary alkyl halide, not te ...
19-3-2013 at 13:34
by: Prometheus23
Benzylamine Hydrochloride to Benzylamine
Oh I see. Well in that case nevermind, I was mistaken and those questions should be in separate thre ...
16-3-2013 at 12:11
by: Prometheus23
Benzylamine Hydrochloride to Benzylamine
Yes I know that the glyoxime isn't used directly for the synthesis of HNIW. I meant that presumably ...
16-3-2013 at 11:53
by: Prometheus23
Benzylamine Hydrochloride to Benzylamine
First of all you probably should have asked this question in the same thread you just started about ...
16-3-2013 at 11:44
by: Prometheus23
Metal/acid reduction of benzoin
I carried out the procedure again but this time with only benzoin and 85% formic acid. The formic ac ...
12-3-2013 at 02:08
by: Prometheus23
How long to heat NaHCO3 to make Na2CO3
As NaHCO3 decomposes into Na2CO3 it gives of water and carbon dioxide. You'll see puffs of gas start ...
10-3-2013 at 06:45
by: Prometheus23
Metal/acid reduction of benzoin
The reduction of benzoin with formic acid was attempted using denatured ethanol as cosolvent. 5g of ...
7-3-2013 at 07:52
by: Prometheus23
h3po3
No, phosphoric acid will not generate hydroiodic acid from elemental iodine, because phosphoric acid ...
6-3-2013 at 03:34
by: Prometheus23
Balanced equation for ASA --> SA
Edit: kavu's explanation was just better, and in the interest of keeping this thread clear an concis ...
11-2-2013 at 01:59
by: Prometheus23
Issues with reduction of vanillin
You should be good if you just use enough acid to destroy any excess borohydride and bring the pH do ...
19-1-2013 at 13:06
by: Prometheus23
M-Cresol
Waffle SS you cut my quote short of its full meaning as well as not understanding it. What I said wa ...
16-1-2013 at 16:38
by: Prometheus23
M-Cresol
No, carboxylic acids like benzoic acid will not be reduced directly to the alkane by Sn/HCl or any o ...
15-1-2013 at 15:42
by: Prometheus23
M-Cresol
Instead of nitrating toluene and trying to isolate the small percentage of 3-nitrotoluene produced i ...
14-1-2013 at 15:17
by: Prometheus23
Would like to propose a trade?
I highly doubt you will get anyone on this forum to give you laboratory glassware in exchange for la ...
12-1-2013 at 14:43
by: Prometheus23
Separation of Isopropanol and Ethyl Acetate
Could you not add the mixture to a large volume of water and separate the EtOAc? Isopropanol will pa ...
1-1-2013 at 12:18
by: Prometheus23
New tramadol to M1 ref discovered, EASY
I came across this paper and just happened to remember this thread. For those interested perhaps thi ...
18-11-2012 at 03:27
by: Prometheus23
Primary amine oxidation
Primary amines can be dichlorinated with TCCA in dichloromethane and then reacted with a base such a ...
1-11-2012 at 21:49
by: Prometheus23
Help with nicotine question
White Yeti, I don't understand why you say this survey ranks nicotine's relative addictive potential ...
23-10-2012 at 17:03
by: Prometheus23
Metal/acid reduction of benzoin
Thank you for your contribution to this thread Sydenhams chorea. When I have time I will perform thi ...
22-10-2012 at 17:49
by: Prometheus23
Help with nicotine question
Nicotine is not the "most addictive substance we currently know of". Such a claim is also often made ...
22-10-2012 at 14:46
by: Prometheus23
Metal/acid reduction of benzoin
If I remember correctly hydrobenzoin in a pinacol rearrangement should give chiefly diphenylacetalde ...
1-7-2012 at 04:55
by: Prometheus23
Metal/acid reduction of benzoin
Thank you Nicodem for your time and effort spent on this research. It is always nice to have another ...
29-6-2012 at 09:29
by: Prometheus23
Metal/acid reduction of benzoin
The product was identified by melting point determination. It gave a melting point of 55-56°C. I su ...
26-6-2012 at 02:37
by: Prometheus23
Balancing
Actually I believe the balanced reaction should be as follows:

CuSO4 + 2 NaHCO3 ==> CuCO3 + Na ...
23-6-2012 at 18:26
by: Prometheus23
Metal/acid reduction of benzoin
Just wanted to report on the success of this procedure. The zinc/acetic acid reduction was tried aga ...
21-6-2012 at 22:31
by: Prometheus23
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