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Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
Nicodem, first of all thank you for taking the time to write such a lengthy critique. I do understan ... |
26-8-2010 at 01:50
by: Quantum_Dom |
Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
[rquote=186171&tid=14326&author=roamingnome]@ Quantum_Dom
you said you used you used DL ... |
25-8-2010 at 17:51
by: Quantum_Dom |
Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
Looks good  . Im suprised how clean you post-reaction is though  . It seems clearer than mine but ... |
25-8-2010 at 12:57
by: Quantum_Dom |
Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
[rquote=186151&tid=14326&author=Methyl.Magic]ok thansk for the info, I understood you used A ... |
25-8-2010 at 11:20
by: Quantum_Dom |
Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
[rquote=186146&tid=14326&author=Methyl.Magic]The color of my solution is darker (amber-like) ... |
25-8-2010 at 11:05
by: Quantum_Dom |
Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
[rquote=186142&tid=14326&author=Methyl.Magic]Today I started your method today, I used 5.3 e ... |
25-8-2010 at 10:47
by: Quantum_Dom |
Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
[rquote=186092&tid=14326&author=percholator]Thanks! I will definitely familiarize myself wit ... |
24-8-2010 at 13:19
by: Quantum_Dom |
Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
[rquote=186087&tid=14326&author=percholator]Correct me if I'm wrong (I cannot easily find cr ... |
24-8-2010 at 12:59
by: Quantum_Dom |
Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
[rquote=186081&tid=14326&author=percholator]Sorry, a bit of a novice here. (And sorry if a b ... |
24-8-2010 at 12:25
by: Quantum_Dom |
Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
[rquote=186060&tid=14326&author=Melgar]Awesome! I can see QD's annoyance at arguing on the ... |
24-8-2010 at 08:30
by: Quantum_Dom |
Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
[rquote=185697&tid=14326&author=Ephoton]hmmm goodbye darzen  [/rquote]
LOL why ? Yield- ... |
20-8-2010 at 05:07
by: Quantum_Dom |
Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
[rquote=185693&tid=14326&author=12332123]This is really great, but could you please quickly ... |
20-8-2010 at 05:00
by: Quantum_Dom |
Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
[quote]
You're really touchy. I'm not attacking you personally, just chill out and address the po ... |
18-8-2010 at 12:59
by: Quantum_Dom |
Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
[rquote=185520&tid=14326&author=DDTea]
If you're not sure that PPA*alaninate is being form ... |
18-8-2010 at 11:13
by: Quantum_Dom |
Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
[rquote=185516&tid=14326&author=DDTea]
So, the burden of proof is still on you to show th ... |
18-8-2010 at 10:52
by: Quantum_Dom |
Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
[rquote=185513&tid=14326&author=DDTea]Sorry I goofed; I meant the alaninate salt.
What ... |
18-8-2010 at 10:39
by: Quantum_Dom |
Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
[rquote=185510&tid=14326&author=DDTea]
One of your suggestions is that a portion of your ... |
18-8-2010 at 10:19
by: Quantum_Dom |
Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
[rquote=185505&tid=14326&author=Methyl.Magic]Very nice work thanks 
The report is compl ... |
18-8-2010 at 09:58
by: Quantum_Dom |
Improvement in the yield of racemic PPA*HCl via Akabori reaction (35 % molar)
[i]This thread is dedicated to those who do desktop research and solely base theyre argument on theo ... |
17-8-2010 at 21:24
by: Quantum_Dom |
Amino alcohol via Akabori, trial run
[rquote=160749&tid=5979&author=manimal]Has anyone actually performed a rigourous analysis of ... |
23-7-2010 at 19:43
by: Quantum_Dom |
Nitroethane from alpha-alanine ?
[quote][i]Originally posted by Ebao-lu[/i]
[quote]Also, the diazonium salt does not decompose becau ... |
2-1-2009 at 10:18
by: Quantum_Dom |
Preparation of methyl tosylate, safe methylating agent
Very nice job spark
[Edited on 31-12-2008 by Quantum_Dom] |
31-12-2008 at 08:35
by: Quantum_Dom |
Preparation of methyl tosylate, safe methylating agent
Klute, I dont know if you were aware of the following procedure but I will post it for information p ... |
31-12-2008 at 07:59
by: Quantum_Dom |
Nitroethane from alpha-alanine ?
[quote][i]Originally posted by McLovin382[/i]
Yay for amines and nitro compounds from amino acids!
... |
30-12-2008 at 21:25
by: Quantum_Dom |
Preparation of methyl tosylate, safe methylating agent
[quote][i]Originally posted by grind[/i]
Tosylate esters are strong cancerogens, like most alkylati ... |
30-12-2008 at 15:54
by: Quantum_Dom |
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