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1,2 dichloroethane synthesis
I cant speak on the effect of impurities, since i used distilled glycol. But the way i did it was th ...
25-10-2021 at 11:20
by: RustyShackleford
1,2 dichloroethane synthesis
as far as i know its not possible to create it from ethylene glycol, atleast by reasonable reagents. ...
25-10-2021 at 10:28
by: RustyShackleford
Setups for burning liquid form aromatic waste
[rquote=664864&tid=157886&author=Tsjerk]Can't you evaporate? Quantities < 100 ml would be ...
5-9-2021 at 03:24
by: RustyShackleford
Setups for burning liquid form aromatic waste
Im looking for a nice way of burning small to medium amounts of aromatic waste, 10-100ml type amount ...
3-9-2021 at 08:27
by: RustyShackleford
preparation of barbituric acid (question about the mechanism)
1. Neutralize the product and catalyze the reaction
2. unlikely, possibly to some degree with a hyd ...
1-9-2021 at 12:47
by: RustyShackleford
Violuric acid salts (fantastic colors and variety)
Hello everyone! Im back with another few violurates to add to this growing collection.
Thanks to O ...
31-8-2021 at 08:33
by: RustyShackleford
What to do with my Ammonium Bicarbonate?
Q1: yes, ive been able to store it for years in a jam jar
Q2: ~15-20%
if you add a solution of so ...
29-8-2021 at 02:46
by: RustyShackleford
Preparation of Bromine
[rquote=663623&tid=13104&author=Keras][rquote=663621&tid=13104&author=Tsjerk]Yes, so ...
5-8-2021 at 14:15
by: RustyShackleford
Preparation of Bromine
[rquote=663610&tid=13104&author=Keras][rquote=663609&tid=13104&author=RustyShacklefo ...
5-8-2021 at 14:13
by: RustyShackleford
Preparation of Bromine
Oxone works very well. I obtained an 88% yield using: 50g NaBr, 80g oxone and 60g 50% sulfruric acid ...
5-8-2021 at 04:12
by: RustyShackleford
Violuric acid salts (fantastic colors and variety)
[rquote=663350&tid=156755&author=woelen]My barbituric acid arrived :)
Next weekend I want t ...
29-7-2021 at 03:57
by: RustyShackleford
Violuric acid salts (fantastic colors and variety)
[rquote=663051&tid=156755&author=woelen]I finally ordered some barbituric acid (from S3 chem ...
19-7-2021 at 16:39
by: RustyShackleford
HCl + Cu + KClO4 odd reaction
Its due to a mixture of copper 1+ and copper 2+. If you bubble air through it (with HCl still in the ...
18-7-2021 at 08:39
by: RustyShackleford
Oxalyl Chloride Challenge
[rquote=662563&tid=82462&author=Praxichys]My lab is being moved but there is a lot of promis ...
13-7-2021 at 05:11
by: RustyShackleford
Violuric acid salts (fantastic colors and variety)
[rquote=662543&tid=156755&author=j_sum1]I am loving this project -- at least watching from t ...
7-7-2021 at 13:12
by: RustyShackleford
Preparation of 3-cyanopropanoic acid from MSG (TCCA oxidative decarboxylation)
[rquote=662556&tid=157679&author=Boffis]Hi Rusty, Nice work and a good write up. I have trie ...
7-7-2021 at 09:26
by: RustyShackleford
Preparation of 3-cyanopropanoic acid from MSG (TCCA oxidative decarboxylation)
[rquote=662538&tid=157679&author=Metacelsus]Can you get a melting point just to check? Possi ...
7-7-2021 at 09:21
by: RustyShackleford
Preparation of 3-cyanopropanoic acid from MSG (TCCA oxidative decarboxylation)
After seeing Bofis 2014 thread on TCCA oxidation of alpha-aminoacids to nitriles, i knew i had to tr ...
6-7-2021 at 13:07
by: RustyShackleford
Violuric acid salts (fantastic colors and variety)
Update on the subject of violuric acid:

Thanks to the help of PoorMans Chemist (who i sent some ...
6-7-2021 at 12:07
by: RustyShackleford
Identification of mist from a leaking/gassing acid bottle
I have seen that in another persons storage with nitric acid (and also in separate incident with HCl ...
28-5-2021 at 15:47
by: RustyShackleford
Salt amoniac sublimation, best method???
Its not a sublimation, you are forming two separate gases that re-react to form NH4Cl.
NH4Cl(s) -& ...
14-5-2021 at 04:37
by: RustyShackleford
Water pumps for Distilation
I have been using these small 5 dollar 12VDC cube pumps for years. so far ive only replaced it once, ...
12-5-2021 at 15:11
by: RustyShackleford
Aspirator vacuum pump
Melkor you are the 5th person ive seen create such a setup and get bad performance. Personally my se ...
12-5-2021 at 15:01
by: RustyShackleford
Extraction of urea CO(NH2)2 from DEF (diesel exhaust fluid) – AdBlue
Overheating is very likely the cause of the ammonia smell. When evaporated AdBlue i boiled it in a l ...
28-4-2021 at 08:28
by: RustyShackleford
Synthesis checks for HMTD
12% peroxide definitely works, but its quite low yield, but that doesnt matter so much since you sho ...
18-4-2021 at 08:24
by: RustyShackleford
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