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Reactions with sodium benzoate
Use it to make benzene, its a pretty straight forward synthesis and benzene ist about the most valua ... |
28-6-2010 at 22:52
by: Taoiseach |
Quinone to make Energetic Compound
p-benzoquinone can be made from OTC precursors:
https://www.sciencemadness.org/whisper/viewthread ... |
28-6-2010 at 22:43
by: Taoiseach |
Exotic Hypochlorites and Chlorites
Anhydrous Sodium hypochlorite can be made but it is only stable at low temperatures. Its an explosiv ... |
9-6-2010 at 23:03
by: Taoiseach |
Copper hydroxide by electrolysis
>Is it true that having copper compounds in ammonia and nitrate solutions can lead to the formati ... |
1-6-2010 at 09:14
by: Taoiseach |
Preparation of cyanides
Well NaCN is slightly more soluble in water than KCN so maybe I should try the sodium salt next time ... |
18-5-2010 at 10:39
by: Taoiseach |
Preparation of cyanides
Thx for the answer Polverone. How much water/EtOH did you use and what temperature? I calculated the ... |
17-5-2010 at 21:31
by: Taoiseach |
Preparation of cyanides
I recently tried the C reduction of potassium cyanate, made by fusing K2CO3 with urea. The fused mas ... |
17-5-2010 at 09:11
by: Taoiseach |
Does Ethanole react with NaClO3-solution ?
Simply boil down the solution. The NaCl will precipate first. You need to filter the solution boling ... |
7-5-2010 at 09:36
by: Taoiseach |
How we could synthesis and stabilized Cu2O
I wonder if it could be useful to reduce nitrate to nitrite... at least its insoluble and the oxidat ... |
4-5-2010 at 09:21
by: Taoiseach |
Highly concentrated H2O2 by extraction with CCl2H2
@franklyn
Fascinating stuff you found there! I have ~500g of urea peroxide, gonna try that extrac ... |
30-4-2010 at 12:19
by: Taoiseach |
Synthesis of Potassium Dichromate
Yes it is 
You can mix iron sulfate or iron powder with potassium chlorate. After fusing the mi ... |
23-4-2010 at 13:03
by: Taoiseach |
Synthesis of Potassium Dichromate
Cr2O3 is a catalyst in the thermal decomposition of chlorate. At just 200°C the yield of dichromate ... |
23-4-2010 at 09:56
by: Taoiseach |
Preparation of cyanides
I didnt control temperature. Literature says it can be destilled from the mixture at 100°C. Also th ... |
9-4-2010 at 07:47
by: Taoiseach |
Preparation of cyanides
I recently mixed together potassium ferricyanide (or was it ferro - well the yellow stuff anyways) w ... |
7-4-2010 at 22:01
by: Taoiseach |
making SCl2 From TCCA-Na2S,possible or not?
Nice job!
What solvent did you use?
I wonder how to best separate the SCl2. |
7-4-2010 at 21:58
by: Taoiseach |
making SCl2 From TCCA-Na2S,possible or not?
Well SCl2 is volatile while the sodium cyanurates are not... its definetely worth a try! The problem ... |
1-4-2010 at 12:16
by: Taoiseach |
Bromine Source and Synthesis
There's certainly no advantage over Painkilla's method of producing the chlorine in situ from HCl an ... |
22-3-2010 at 00:08
by: Taoiseach |
Preparation of elemental phosphorus
[rquote=173361&tid=65&author=Magpie]It seems like all home chemists wore ties in the old day ... |
10-3-2010 at 04:29
by: Taoiseach |
Sulfuric acid and toner
Heating & much stirring will certainly speed it up. I was suprised myself how fast copper dissol ... |
7-3-2010 at 03:59
by: Taoiseach |
Sulfuric acid and toner
You could try tetramminecopper(II)hydroxide to dissolve the paper. It is known to dissolve cellulose ... |
6-3-2010 at 14:37
by: Taoiseach |
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
Yes could be impure. I gotta test this with pure 5-AZT again and see if I get the same result.
Bu ... |
18-2-2010 at 06:27
by: Taoiseach |
5-ATZ(5-Aminotetrazole), the nitrotetrazolate ion and friends
I recently prepared some 5-aminotetrazole (5-ATZ). After leaving the solution for 2 days, no more cr ... |
17-2-2010 at 01:19
by: Taoiseach |
Hydrazine
Damn I can't wait to know if this method really works 
Just heat the damn stuff somehow... put ... |
11-2-2010 at 09:23
by: Taoiseach |
Hydrazine
>are there some more?
If you had read my post above you wouldn't ask: HEAT IT.
If it leaves a ... |
11-2-2010 at 08:03
by: Taoiseach |
Hydrazine
I really enjoy your experimental reports Myfanwy, its always something interesting
>when i ... |
10-2-2010 at 13:08
by: Taoiseach |
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