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Preparation of Benzoin
I like the write up Magpie, I have run this reaction multiple times on approximately 100 grams of be ... |
11-3-2012 at 00:17
by: benzylchloride1 |
Synthesis of bourgeonal
Here is a prep of p-tert-butylbromobenzene:
In a 3-liter, three-necked flask equipped with a mechan ... |
15-2-2012 at 22:58
by: benzylchloride1 |
Synthesis of bourgeonal
Another possibility would be to run a Kumada-type coupling of allyl magnesium bromide with 4-bromo-t ... |
14-2-2012 at 22:34
by: benzylchloride1 |
Please welcome our latest moderator, ScienceSquirrel
Bravo ScienceSquirrel! |
13-2-2012 at 00:14
by: benzylchloride1 |
Russian HyperLab: reformed and renewed
[quote]
Of course it is not wise to be associated with anything at all as far as your professor g ... |
13-2-2012 at 00:03
by: benzylchloride1 |
Preparation of Styrene and Phenylacetylene from Polystyrene
Nice synthesis, reminds me of some good times in my own lab several years ago. I used styrofoam as t ... |
1-2-2012 at 21:41
by: benzylchloride1 |
Purification of Toluene
I use Ace Hardware toluene for all of my syntheses. I always distill about 25 mL of the solvent,the ... |
1-2-2012 at 21:22
by: benzylchloride1 |
Strike?
This about sums it up:
Once the religious, the hunted and weary
Chasing the promise of freedom a ... |
17-1-2012 at 22:18
by: benzylchloride1 |
Does this company sell to individuals?
The crazy thing about Sigma Aldrich was that it was started by Alfred Bader in a garage. One of the ... |
12-1-2012 at 23:35
by: benzylchloride1 |
The Synthesis of Nickelocene
I have also prepared cobaltocene, titanocene dichloride and ferrocene by similar methods. Anhydrous ... |
4-1-2012 at 21:01
by: benzylchloride1 |
The Synthesis of Nickelocene
[quote]
Wish I had the setup to do this, wanted to do it for a long time.
Take a look at the Ino ... |
3-1-2012 at 20:52
by: benzylchloride1 |
The Synthesis of Nickelocene
Synthesis of Nickelocene
Introduction:
Bis(cyclopentadienyl)nickel(II) or nickelocene is a wid ... |
2-1-2012 at 22:55
by: benzylchloride1 |
Alternative inert gasses
i use a Air Liquide cylinder of compressed balloon grade helium for all of my reactions that have to ... |
2-1-2012 at 11:40
by: benzylchloride1 |
UCLA prof and UC system face felony charges after lab accident
Tert-butyl lithium is very pyrophoric, I have handled the stuff before and it can be quite scary. Th ... |
1-1-2012 at 21:18
by: benzylchloride1 |
Total Synthesis of Carpanone from Catechol
I have been gradually working on the carpanone synthesis, but grad school has slowed down my progres ... |
1-1-2012 at 20:42
by: benzylchloride1 |
Pretty Pictures (1)
I obtain many chemicals off of Ebay, and I also know someone that I can buy chemicals through. I am ... |
1-1-2012 at 20:18
by: benzylchloride1 |
Pretty Pictures (1)
Here is some pictures of a nickelocene, bis(cyclopentadienyl)nickel(II) synthesis I conducted at my ... |
1-1-2012 at 18:59
by: benzylchloride1 |
Tour My Lab
Most of the equipment is in working order, the 1310 IR and both UV-Vis spectrophotometers run. The 4 ... |
24-12-2011 at 22:51
by: benzylchloride1 |
Buchi Screw Wheel 00565 needed!
Check Buchi's Amazon store, I bought one of these from them. Expect about $100 with shipping for a n ... |
18-12-2011 at 22:49
by: benzylchloride1 |
Extraction of terpenes from eucalyptus and conversion to p-cymene
I love terpenes! Sounds like a good experiment, I would buy some eucalyptus oil, since the amount ob ... |
8-12-2011 at 23:25
by: benzylchloride1 |
Tour My Lab
The balance table is a spare butchers block, it works pretty well. I am a big fan of the old Mettler ... |
8-12-2011 at 23:06
by: benzylchloride1 |
Tour My Lab
I ran out of space, here is my oldest gas chromatograph and the crown jewel, my Hitachi R 1200 60 MH ... |
7-12-2011 at 23:29
by: benzylchloride1 |
Tour My Lab
Here is a semi-complete tour of my lab, several new instruments are missing
[file]16760[/file] ... |
7-12-2011 at 23:14
by: benzylchloride1 |
Does anyone have a Hitachi R 1200 NMR spectrometer that they would be interested in selling
Here are a few pictures of my new NMR spectrometer. The shunt key, and other accessories arrived y ... |
7-12-2011 at 23:04
by: benzylchloride1 |
Does anyone have a Hitachi R 1200 NMR spectrometer that they would be interested in selling
I paid $500 for the instrument I purchased. All of the electronics work, I am now waiting to get a s ... |
30-11-2011 at 12:15
by: benzylchloride1 |
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