Sciencemadness Discussion Board
Not logged in [Login - Register]
Go To Bottom

Search
[Next Page]
Preparation of Benzoin
I like the write up Magpie, I have run this reaction multiple times on approximately 100 grams of be ...
11-3-2012 at 00:17
by: benzylchloride1
Synthesis of bourgeonal
Here is a prep of p-tert-butylbromobenzene:
In a 3-liter, three-necked flask equipped with a mechan ...
15-2-2012 at 22:58
by: benzylchloride1
Synthesis of bourgeonal
Another possibility would be to run a Kumada-type coupling of allyl magnesium bromide with 4-bromo-t ...
14-2-2012 at 22:34
by: benzylchloride1
Please welcome our latest moderator, ScienceSquirrel
Bravo ScienceSquirrel!
13-2-2012 at 00:14
by: benzylchloride1
Russian HyperLab: reformed and renewed

[quote]
Of course it is not wise to be associated with anything at all as far as your professor g ...
13-2-2012 at 00:03
by: benzylchloride1
Preparation of Styrene and Phenylacetylene from Polystyrene
Nice synthesis, reminds me of some good times in my own lab several years ago. I used styrofoam as t ...
1-2-2012 at 21:41
by: benzylchloride1
Purification of Toluene
I use Ace Hardware toluene for all of my syntheses. I always distill about 25 mL of the solvent,the ...
1-2-2012 at 21:22
by: benzylchloride1
Strike?
This about sums it up:

Once the religious, the hunted and weary
Chasing the promise of freedom a ...
17-1-2012 at 22:18
by: benzylchloride1
Does this company sell to individuals?
The crazy thing about Sigma Aldrich was that it was started by Alfred Bader in a garage. One of the ...
12-1-2012 at 23:35
by: benzylchloride1
The Synthesis of Nickelocene
I have also prepared cobaltocene, titanocene dichloride and ferrocene by similar methods. Anhydrous ...
4-1-2012 at 21:01
by: benzylchloride1
The Synthesis of Nickelocene

[quote]
Wish I had the setup to do this, wanted to do it for a long time.
Take a look at the Ino ...
3-1-2012 at 20:52
by: benzylchloride1
The Synthesis of Nickelocene

Synthesis of Nickelocene

Introduction:
Bis(cyclopentadienyl)nickel(II) or nickelocene is a wid ...
2-1-2012 at 22:55
by: benzylchloride1
Alternative inert gasses
i use a Air Liquide cylinder of compressed balloon grade helium for all of my reactions that have to ...
2-1-2012 at 11:40
by: benzylchloride1
UCLA prof and UC system face felony charges after lab accident
Tert-butyl lithium is very pyrophoric, I have handled the stuff before and it can be quite scary. Th ...
1-1-2012 at 21:18
by: benzylchloride1
Total Synthesis of Carpanone from Catechol
I have been gradually working on the carpanone synthesis, but grad school has slowed down my progres ...
1-1-2012 at 20:42
by: benzylchloride1
Pretty Pictures (1)
I obtain many chemicals off of Ebay, and I also know someone that I can buy chemicals through. I am ...
1-1-2012 at 20:18
by: benzylchloride1
Pretty Pictures (1)
Here is some pictures of a nickelocene, bis(cyclopentadienyl)nickel(II) synthesis I conducted at my ...
1-1-2012 at 18:59
by: benzylchloride1
Tour My Lab
Most of the equipment is in working order, the 1310 IR and both UV-Vis spectrophotometers run. The 4 ...
24-12-2011 at 22:51
by: benzylchloride1
Buchi Screw Wheel 00565 needed!
Check Buchi's Amazon store, I bought one of these from them. Expect about $100 with shipping for a n ...
18-12-2011 at 22:49
by: benzylchloride1
Extraction of terpenes from eucalyptus and conversion to p-cymene
I love terpenes! Sounds like a good experiment, I would buy some eucalyptus oil, since the amount ob ...
8-12-2011 at 23:25
by: benzylchloride1
Tour My Lab
The balance table is a spare butchers block, it works pretty well. I am a big fan of the old Mettler ...
8-12-2011 at 23:06
by: benzylchloride1
Tour My Lab
I ran out of space, here is my oldest gas chromatograph and the crown jewel, my Hitachi R 1200 60 MH ...
7-12-2011 at 23:29
by: benzylchloride1
Tour My Lab
Here is a semi-complete tour of my lab, several new instruments are missing

[file]16760[/file] ...
7-12-2011 at 23:14
by: benzylchloride1
Does anyone have a Hitachi R 1200 NMR spectrometer that they would be interested in selling

Here are a few pictures of my new NMR spectrometer. The shunt key, and other accessories arrived y ...
7-12-2011 at 23:04
by: benzylchloride1
Does anyone have a Hitachi R 1200 NMR spectrometer that they would be interested in selling
I paid $500 for the instrument I purchased. All of the electronics work, I am now waiting to get a s ...
30-11-2011 at 12:15
by: benzylchloride1
[Next Page]

  Go To Top