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Prototocatechualdehyde methylenation. Photo-essay.
Wouldn't the yield be higher if less quantity of aldehyde is used? Erowid says that this method of m ...
16-9-2018 at 00:28
by: mackolol
demethylation of tryptammonium iodide
ok thanks very much.
12-9-2018 at 10:20
by: mackolol
demethylation of tryptammonium iodide
As i'm going through Shulgin's book TIHKAL for last days i came across DMT synthesis. It is synthesi ...
12-9-2018 at 06:18
by: mackolol
Stupid laws in the European Union.
In Poland Iodine and Red Phosphorus can be easily obtained and are legal even benzaldehyde p fluoro ...
3-9-2018 at 10:58
by: mackolol
Stupid laws in the European Union.
In Poland you can easily buy sulfuric acid and potassium permanganate (in drug store or from chem su ...
3-9-2018 at 08:59
by: mackolol
OTC Oxalyl Chloride Challenge
[rquote=531817&tid=74187&author=AJKOER]First, one may wish to investigate a claim of a succe ...
27-8-2018 at 12:19
by: mackolol
Modified Patent Route to Oxalyl Chloride
[rquote=93950&tid=8291&author=Sauron]

A very likely third route esp for those who can't g ...
27-8-2018 at 08:59
by: mackolol
Synthesis of Sulfur trioxide method proposal
You can also decompose thermally FeSO4 to Fe2O3 SO2 and SO3. It's cheap as dirt and temperature of f ...
23-8-2018 at 03:59
by: mackolol
Synthesis of Sulfur trioxide method proposal
This is much more OTC and easier method for making sulphuric acid.
https://www.youtube.com/watch?v= ...
20-8-2018 at 22:48
by: mackolol
is it possible to make protein from carbohydrate and fats from breathing nitrogen in air?
Nitrogen itself isn't very unreactive. It's role in air is to dilute oxygen (i think) because pure o ...
20-8-2018 at 07:30
by: mackolol
Hydroxylamine alternatives or synthesis
But do oximes also get reduced by Fe(III)? What if we oxidise primary amine -NH2 or imine =NH with F ...
19-8-2018 at 21:57
by: mackolol
storing carborane acid? (or other very strong acids)
Carborane acid isnt corrosive, thats what wikipedia says it's just very strong as an acid which mean ...
19-8-2018 at 13:39
by: mackolol
Hydroxylamine alternatives or synthesis
But AJKOER does it necessarily need two radicals nh2 and oh? Isn't hydroxyl radical reactive enough ...
19-8-2018 at 13:31
by: mackolol
Metabisulfite for Bisulfite Adduct Discussion
I think he wants to get rid of ketones in his thinner and leave unreacted thf JJay
19-8-2018 at 06:54
by: mackolol
Hydroxylamine alternatives or synthesis
This site presents a lot of ways to oxidise primary amine to oxime for example with meta- Chloropero ...
19-8-2018 at 06:02
by: mackolol
Hydroxylamine alternatives or synthesis
Hydroxyl radical can be generated by Fenton's reagent. It's just feso4 solution mixed with h2o2. But ...
19-8-2018 at 05:51
by: mackolol
Hydroxylamine alternatives or synthesis
Look at this. Is seems you can reduce nitroalkene with na2s2o4 or (i believe) using Thiourea dioxide ...
19-8-2018 at 04:38
by: mackolol
anyone have experience forming grignards from chlorobenzene
Maybe try in dioxane it's cheap as dirt and since it's cyclic same as thf it would work well.
14-8-2018 at 07:52
by: mackolol
Just type in google "synthesis of acetylene" found it on first found website
F is a wide-necked 250 ml bolt-head flask, to which is fitted a double-surface reflux water-condense ...
14-8-2018 at 00:36
by: mackolol
The Short Questions Thread (4)
No it won't. Even in some procedures it says that you use "tetrahydrofuran freshly distilled from so ...
13-8-2018 at 01:05
by: mackolol
What can I do with Sulphur Dioxide gas ?
You can make some sulphuric acid by the copper chloride process, which NurdRage presented in one of ...
12-8-2018 at 04:03
by: mackolol
HNO3 from Ca(NO3)2 + HCl - any reason it wouldn't work?
With Muriatic acid it won't work as Hcl is gas and its way more volatile than hno3. Hcl boils at muc ...
20-7-2018 at 23:00
by: mackolol
How do you clean stubbornly dirty glassware when no solvent seems to work?
In most cases usual 98% sulphuric acid does the job. You can heat it if seems to not work. Also you ...
20-7-2018 at 03:33
by: mackolol
The Short Questions Thread (4)
Is there any reagent that helps detecting oximes in mixture? (changes color if oxime is present)
19-7-2018 at 03:32
by: mackolol
Thiourea Dioxide --> better than borohydride?
Does anybody have an access to document "Reduction of Organic Compounds with Thiourea Dioxide II. Th ...
27-6-2018 at 05:12
by: mackolol
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