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Nickel aminoguanidine diperchlorate
[rquote=696892&tid=158381&author=Axt]
Solution 1
Displacing AG bicarbonate with hydrochlor ...
27-11-2024 at 08:09
by: pdb
Nickel aminoguanidine diperchlorate
[rquote=696936&tid=158381&author=Laboratory of Liptakov]
Procedure from Ni(NO3)2: 2g Ni(NO3 ...
24-11-2024 at 11:44
by: pdb
Nickel aminoguanidine diperchlorate
This time, I followed example 2.3 from the patent and Microtek's advice:

Synthesis of Hexaammine ...
21-11-2024 at 05:51
by: pdb
Exotic Primaries - Complex Salts
Isn't example 2.4 of patent EP2450330A2 ?
20-11-2024 at 13:17
by: pdb
Nickel aminoguanidine diperchlorate
After 2 hours, red needles appeared on the surface. I will retry the ultrasonic bath.

Meanwhile, ...
20-11-2024 at 06:49
by: pdb
Attempt with HClO4
This time, I tried the synthesis with HClO4. Nickel perchlorate hexahydrate is synthesized in situ, ...
20-11-2024 at 06:09
by: pdb
Exotic Primaries - Complex Salts
[rquote=696827&tid=1778&author=Axt]Good god pdb, it's been just shy of 20 years it's good to ...
18-11-2024 at 12:50
by: pdb
Exotic Primaries - Complex Salts
[rquote=696793&tid=1778&author=greenlight]
We do have some theories on the DDT transition. ...
17-11-2024 at 14:53
by: pdb
Dinitro-benzenediazonium perchlorate
I hesitated to include it in my list of primaries because I’ve never managed to achieve DDT in ope ...
17-11-2024 at 14:39
by: pdb
Nickel aminoguanidine diperchlorate
[rquote=696803&tid=158381&author=Laboratory of Liptakov]NH4ClO4 from HClO4 + NH4OH ? It sho ...
17-11-2024 at 12:14
by: pdb
Long life, short list



Energetic materials have been a hobby of mine for several decades. Especially primary explosiv ...
17-11-2024 at 08:05
by: pdb
uNAP failure
I meticulously followed Hey Buddy's recipe:


1 g of aminoguanidine bicarbonate
0.86 g of NH4ClO ...
17-11-2024 at 07:51
by: pdb
Cutting with primary
The PIB is incorporated in the usual way: dissolved in gasoline, but without oil. The hardest part i ...
28-3-2023 at 12:06
by: pdb
Cutting with primary
Sorry guys, but I had to delete some recent data for some reasons. This makes the thread a bit shaky ...
13-3-2023 at 05:51
by: pdb
Cutting with primary
Nitrobenzenediazonium perchlorate, 50 mg + 4 mg PIB. In my experience, it is by far the most powerfu ...
11-3-2023 at 15:22
by: pdb
Measuring VOD
Synchronising measuring instruments such as oscilloscopes with such fast phenomena is not easy. Here ...
9-2-2022 at 13:27
by: pdb
Cutting with primary
This time I shot the back of the Bristol to avoid the camera being blinded by the flash of the deton ...
30-11-2021 at 02:32
by: pdb
Cutting with primary
Again, the nitrobenzenediazonium perchlorate provides a beautiful image, captured at 240 fps. I thi ...
24-11-2021 at 14:03
by: pdb
Trial with (NCN3)3
This time I tried to form a trail of CTA (cyanuric triazide) by melting (m.p. 94°).But once liquid, ...
2-11-2021 at 08:36
by: pdb
Cutting with AgN3
The same cutting experiment with AgN3 does not work well: the size of the crystals (much larger than ...
26-10-2021 at 02:02
by: pdb
Cutting with primary
The plexiglass assembly consists, from top to bottom, of a sheet of explosive (PETN preferable becau ...
23-10-2021 at 01:39
by: pdb
Cutting with primary
[rquote=666460&tid=158024&author=katyushaslab]nitrobenzenediazonium perchlorate? Is that the ...
22-10-2021 at 07:29
by: pdb
Cutting with primary
[rquote=666444&tid=158024&author=Laboratory of Liptakov]Finally someone with Art of primary ...
21-10-2021 at 22:59
by: pdb
Cutting with primary
Next try with a 41 cm path. Photo quality is poor due to lack of light.


[file]90631[/file] [fi ...
21-10-2021 at 07:36
by: pdb
Cutting with primary
Cutting test of bristol board with a primary explosive.The primer is nitrobenzenediazonium perchlora ...
21-10-2021 at 06:56
by: pdb
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