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Aminorex Synth
many of us would be too happy to have such a good source :P so i would suggest you to get proper lab ...
28-6-2007 at 18:51
by: tr41414
Aminorex Synth
The akabori is extremely low yielding I think (tribute to CycloKnight for doing it and posting those ...
28-6-2007 at 00:56
by: tr41414
Playing with tyrosine
If you look closer, you would see that the reactions i posted are different, all starting from tyros ...
28-6-2007 at 00:22
by: tr41414
Playing with tyrosine
I just happen to have 100g of quite pure tyrosine (USP, label says 100% !?)... It's one of most easi ...
27-6-2007 at 12:30
by: tr41414
Aminorex Synth
There are many, many ways to PPA and the aminorex (via styrene oxide, p1p-ol, akabori or maybe cath ...
27-6-2007 at 08:32
by: tr41414
Aminorex Synth
;) you would get n-mar instead of 4-mar... dunno if it is of any pharmachological significance... an ...
26-6-2007 at 03:44
by: tr41414
Aminorex Synth
hmm... aminorex & friends have been banned mainly because they tend to produce hart problems in ...
23-6-2007 at 13:38
by: tr41414
Acetylene Synth
Hmm... carbide must be out there (just go asking around in hardware-shop, say you have an old acetyl ...
5-6-2007 at 13:21
by: tr41414
Ideas for making ethylenediamine?
If working the glycol + urea seems a very good method... Any references on synthesis of other alkyla ...
31-5-2007 at 12:24
by: tr41414
Ideas for making ethylenediamine?
I have a feeling that it will be hard to obtain ethylene dichloride from glycol... More likely chlor ...
31-5-2007 at 07:26
by: tr41414
PEA and mek -> NPP?
i think you are confusing two different reactions. one is the known-to-work divinyl ketone + MeAm, w ...
29-5-2007 at 09:54
by: tr41414
Cinnamaldehyde as Insecticide/Fungicide
Cinnamaldehyde seems to be safe for use, but i have some doubts that eugenol would go as an insect r ...
26-5-2007 at 12:49
by: tr41414
PEA and mek -> NPP?
Actually the reaction between acetone, methylamine and formaldehyde has been documented, and it does ...
26-5-2007 at 12:37
by: tr41414
PEA and mek -> NPP?
There seem to be only 3 threads on the hive regarding this way of 4-piperidone synthesis:

ning: O ...
24-5-2007 at 10:49
by: tr41414
PEA and mek -> NPP?
sorry... have no references on that... but it would be the simplest of 4-piperidone synthesis and se ...
24-5-2007 at 09:55
by: tr41414
PEA and mek -> NPP?
just an idea - what about using glyoxylic acid or it's esters instead of formaldehyde? not as readil ...
24-5-2007 at 09:28
by: tr41414
PEA and mek -> NPP?
The disscussion on the hive seemed not to give any conclusive results. But as this reaction is not m ...
24-5-2007 at 09:13
by: tr41414
Phenyl alkyl ketone synthesis
Does anyone have any reference to synthesis of 3,4,5-trimethoxyphenyl amyl ketone?

Probably the s ...
23-5-2007 at 13:28
by: tr41414
Aromatic modification of phenylpiperazine
I have gotten my hands on some n-phenylpiperazine and was searching for procedures on modifying the ...
14-12-2006 at 12:39
by: tr41414
Willgerodt rxn: Styrene monomer -> phenylacetamide
I think it's thinner for some kind of polystyrene based car color or sth. like that...
Don't know e ...
21-11-2006 at 22:01
by: tr41414
Willgerodt rxn: Styrene monomer -> phenylacetamide
kmno4:

Literature gives divided reports on efficancy of reaction... But hey... 50% isn't so bad.. ...
12-11-2006 at 10:21
by: tr41414
Cyanate substitutes for CBrN
You are probably refering to reaction PPA >> 4-MAR. People are usualy not very happy to search ...
20-9-2006 at 13:02
by: tr41414
High temperature reaction vessel
I couldn't find the patent 832,096 LONDON on B2O3+NaCl reaction, but maybe substitution of NaCl with ...
17-9-2006 at 09:44
by: tr41414
PhCH2NO2 from PhCH2OH
I belive that PhCH2OH + HCl > PhCH2Cl + H2O, PhCH2Cl + NaNO2 > PhCH2NO2 + PhCH2ONO (byproduct) ...
16-9-2006 at 14:42
by: tr41414
Naloxone & friends
I just found the post i was reffering to. Here is just a part on BCl3 production.

[quote][i]TheHi ...
16-9-2006 at 13:03
by: tr41414
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