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Xylene failed to separate from methanol..Detergent contamination from KOH??
[rquote=318228&tid=28864&author=bfesser] . . .
your solution could be as simple as adding a ...		 7-2-2014 at 06:44
by: zig
Xylene failed to separate from methanol..Detergent contamination from KOH??
Ran into a ridiculous roadblock today..

After running an amalgam on a ketone (with the same old t ...		 7-2-2014 at 04:25
by: zig
help needed with vac distillation of a carbonyl
Figured I'd provide closure for those curious.. after hours of defcon10, painstaking leakproofing th ...		 7-2-2014 at 02:59
by: zig
Prototocatechualdehyde methylenation. Photo-essay.
Excellent write-up cycloknight, love the pics. I'll bet your lab reeked of sunshine and rainbows aft ...		 31-1-2014 at 00:08
by: zig
help needed with vac distillation of a carbonyl
Well now I know there's solvent in the resevoir- lots of fucking water.

Through some unholy mira ...		 30-1-2014 at 15:53
by: zig
help needed with vac distillation of a carbonyl
Holy molybdenum Mr. Acid! Truly you are ghe nunz bunz. I really appreciate you taking the time to ty ...		 29-1-2014 at 10:00
by: zig
help needed with vac distillation of a carbonyl
After refreshing the vacuum oil, the gauge read that it was pulling 21inHg. Which equals, if my math ...		 28-1-2014 at 18:07
by: zig
help needed with vac distillation of a carbonyl
Partial immersion thermometer was set in the vapor zone.
Vac source was attached to a manifold with ...		 27-1-2014 at 15:15
by: zig
help needed with vac distillation of a carbonyl
Hi all,

I've run into some annoying issues whilst trying to vac distill a high boiling carbonyl.
...		 27-1-2014 at 02:45
by: zig

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