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synthesis of methyl iodide from methanol, HCl and sodium iodide?
[rquote=439822&tid=65075&author=DJF90]Is there a rationale behind how you conducted the expe ...
25-2-2016 at 08:09
by: Nicodem
Grignard successes and failures
[rquote=439490&tid=65348&author=fluorescence]40 ml 2.5 M fresh n-Butyl Lithium in Hexane sam ...
25-2-2016 at 07:51
by: Nicodem
synthesis of methyl iodide from methanol, HCl and sodium iodide?
A lot of talk instead of doing an experiment. Like this:

To NaI (18.8 g, 125 mmol) was added meth ...
23-2-2016 at 12:06
by: Nicodem
amide and nitrous acid?
A related topic: [url=https://www.sciencemadness.org/whisper/viewthread.php?tid=12038]Acid halides f ...
15-2-2016 at 08:37
by: Nicodem
Oxidation of styrene to phenylacetaldehyde
Before this end up with unnecessary misunderstanding and accusations...

Neither hydrogen peroxid ...
15-2-2016 at 08:34
by: Nicodem
Friedel-Crafts acylation of aliphatic imines derivatives of amino acids
[quote]lolz I majored in and tutor organic chemistry. I know what I'm talking about.[/quote]
Was th ...
10-2-2016 at 09:20
by: Nicodem
problem of Diketoacid synthesis - starting material regeneration
[rquote=438434&tid=65285&author=clemi2310]I am curious because to do my condensation to form ...
10-2-2016 at 09:13
by: Nicodem
B + HCl
Please do not use google-links! Correct your post and link directly to the site with the proper URL. ...
10-2-2016 at 08:55
by: Nicodem
4-anilino-N-phenethylpiperidine 2-furanamide
Clearly, if you have scientific evidence, you can publish it in scientific journals, assuming it is ...
30-1-2016 at 07:51
by: Nicodem
Methylammonium Acetate - Synthesis of Crystal
[rquote=436209&tid=65104&author=swami.me]Thanks for correcting me. I really don't need large ...
24-1-2016 at 07:56
by: Nicodem
Methylammonium Acetate - Synthesis of Crystal
[rquote=436209&tid=65104&author=swami.me]I am new to organic synthesis. I would like to synt ...
22-1-2016 at 08:53
by: Nicodem
Hydrochlorination of alk-1-ene?
[rquote=436136&tid=64979&author=blogfast25]That paper is very interesting but from what I ca ...
21-1-2016 at 08:43
by: Nicodem
Hydrochlorination of alk-1-ene?
[rquote=435765&tid=64979&author=blogfast25]
.... 2-substituted 1-alkenes (specifically limo ...
21-1-2016 at 07:25
by: Nicodem
Niacin Chlorochromate (NCC??) for oxidation of alcohols
Thanks for sharing your experiment.
[rquote=435675&tid=65067&author=DrDevice]So, I have spe ...
21-1-2016 at 07:22
by: Nicodem
Hydrochlorination of alk-1-ene?
[rquote=434989&tid=64979&author=blogfast25]But wouldn't hydrolysis [i]in mild conditions[/i] ...
12-1-2016 at 09:54
by: Nicodem
Synthesis of longer chain tertiary alcohols
Try stirring a solution of pinenes or limonene in acetic acid in the presence of 1 mol% conc. sulfur ...
12-1-2016 at 09:03
by: Nicodem
Hydrochlorination of alk-1-ene?
[rquote=434907&tid=64979&author=blogfast25]Actually, the molecule I'm considering hydrochlor ...
12-1-2016 at 08:52
by: Nicodem
toluene --> benzaldehyde
The autooxidation of [i]ortho[/i]-nitrotoluene, or the oxidation of its carbonanion by oxygen, can g ...
12-1-2016 at 08:21
by: Nicodem
Hydrochlorination of alk-1-ene?
The [i]Organic Syntheses[/i] example is a Michael addition (1,4-nucleophilic conjugate addition). It ...
11-1-2016 at 12:00
by: Nicodem
Synthesis of longer chain tertiary alcohols
[rquote=434689&tid=15171&author=blogfast25]Trichloroacetic Acid is used there because it's a ...
10-1-2016 at 03:12
by: Nicodem
Preparation of pyrrolidine via decarboxylation of l-proline
Scr0t, I like your report and I hope you don't mind me moving it to Prepublication.
I particularly ...
25-12-2015 at 06:55
by: Nicodem
formaldehyde methylamine and formic acid
[rquote=432798&tid=64797&author=Marcelo F]The mechanism is the Eschweiler–Clarke reaction
...
25-12-2015 at 06:44
by: Nicodem
N-isopropyl-2-propanimine preparation
[rquote=432464&tid=64741&author=gluon47]@nicodem, to answer your original question, no I don ...
23-12-2015 at 00:55
by: Nicodem
N-isopropyl-2-propanimine preparation
[rquote=432364&tid=64741&author=User123]Then he should use IPA.

The purpose of refluxing ...
22-12-2015 at 03:44
by: Nicodem
N-isopropyl-2-propanimine preparation
[rquote=432361&tid=64741&author=User123]Hence I advised him to reflux the toluene to form th ...
22-12-2015 at 03:33
by: Nicodem
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