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How hazardous is fluorine chemistry?
It's a pretty broad question, isn't it? As Texium emphasized, HF is extremely dangerous. Many fluori ... |
14-2-2024 at 11:35
by: clearly_not_atara |
URGENT - To Vesp
https://www.ncbi.nlm.nih.gov/pmc/articles/PMC7304568/
Describes the direct reaction of hydroxylam ... |
13-2-2024 at 06:26
by: clearly_not_atara |
Acetic anhydride preparation
I can't edit that post anymore, but I wanted to add that in the absence of phthalic acid, a high-boi ... |
11-2-2024 at 22:21
by: clearly_not_atara |
Looking for ideas for a new Synthesis Open Access Platform
I think I would avoid trying to be all things to all people. One thing I've thought would be useful ... |
10-2-2024 at 18:23
by: clearly_not_atara |
Acetic anhydride preparation
Loptr: It was discussed on the previous page. In order to better keep track of the enormous amount o ... |
10-2-2024 at 17:30
by: clearly_not_atara |
Acetic anhydride preparation
S2Cl2 is not so bad itself, but it's infamous for ruining any container you keep it in. So you proba ... |
9-2-2024 at 14:22
by: clearly_not_atara |
Acetic anhydride preparation
I just don't think it's considered interesting. Mostly we're interested in preparing acetic anhydrid ... |
9-2-2024 at 08:18
by: clearly_not_atara |
URGENT - To Vesp
Ha! And here I thought I had finally bored everyone to death |
9-2-2024 at 05:48
by: clearly_not_atara |
Questions in electroplating
I'm confused? Isn't the anode supposed to corrode? It's pitting because it's not noble enough to evo ... |
8-2-2024 at 18:58
by: clearly_not_atara |
Detonation Velocity of organic explosive cannot exceed 11 Km/s
It appears that this assertion may have been defeated in an unexpected manner. The novel superhard m ... |
8-2-2024 at 09:14
by: clearly_not_atara |
Can KBH4 substitute NaBH4 in ethanol/methanolic solutions for reduction of ketones to alcohol.
^I think you'd have a better time contributing to the Sciencemadness Wiki. Wikipedia usually wants " ... |
6-2-2024 at 21:06
by: clearly_not_atara |
Praparation of Nitromethane
I think a key reason is that it's the easiest saturated aliphatic nitro compound to make 
Unles ... |
6-2-2024 at 17:57
by: clearly_not_atara |
Eutectic salts for heating bath alternative
Since the methanesulfonates can substitute for nitrate in dissolving silver, I thought I would look ... |
2-2-2024 at 16:21
by: clearly_not_atara |
S2Cl2 by chlorination with CuCl2 in MeCN?
Because of the formation of the acetonitrile-Cu+ complex, copper (II) is more strongly oxidizing in ... |
2-2-2024 at 09:29
by: clearly_not_atara |
A failed attempt at p-hydroxybenzoic acid
Orgsyn says 230 C. Your procedure says 225 F. This discrepancy is alarming.
EDIT: Oh, I see. You ... |
30-1-2024 at 08:47
by: clearly_not_atara |
Synthesis of Chloroacetic acid
You shouldn't need any light with a sulfur catalyst, in this case the mechanism is fully ionic and n ... |
30-1-2024 at 08:45
by: clearly_not_atara |
Can KBH4 substitute NaBH4 in ethanol/methanolic solutions for reduction of ketones to alcohol.
I agree with moving the thread. And the concerns about solid mixtures of borohydride and perchlorate ... |
29-1-2024 at 10:10
by: clearly_not_atara |
Praparation of Nitromethane
My guess is probably not, nitrate is very unreactive to nucleophilic substitution, but I guess I'm h ... |
26-1-2024 at 09:43
by: clearly_not_atara |
UK: Hydrochloric acid, phosphoric acid, and hexamine now restricted/banned!
[rquote=689517&tid=160046&author=Alkoholvergiftung]clearly_not_atara what would be the best ... |
25-1-2024 at 07:33
by: clearly_not_atara |
Can hydrogen peroxide be vacuum distilled straight from sodium percarbonate?
[rquote=690393&tid=160113&author=teodor]But making a solution will spoil the whole process w ... |
24-1-2024 at 06:40
by: clearly_not_atara |
Has anyone dissolved Titanium Dioxide?
Lactic acid can attack TiO2 and forms a soluble complex IIRC. You probably want finely powdered tita ... |
23-1-2024 at 09:15
by: clearly_not_atara |
Can hydrogen peroxide be vacuum distilled straight from sodium percarbonate?
It's not really a concern whether complexes form. The existence of the complex is not the major barr ... |
22-1-2024 at 11:57
by: clearly_not_atara |
Can hydrogen peroxide be vacuum distilled straight from sodium percarbonate?
^ you could also use NaH2PO4 so that the sodium carbonate becomes bicarbonate instead of making lots ... |
20-1-2024 at 09:40
by: clearly_not_atara |
Can hydrogen peroxide be vacuum distilled straight from sodium percarbonate?
You could probably get some decent results with a mixture of water and urea (20-30% urea) at < 0 ... |
20-1-2024 at 08:04
by: clearly_not_atara |
Allophanic acid
I guess you might get somewhere the same way they make carbamate salts, by forming the anion of urea ... |
15-1-2024 at 14:10
by: clearly_not_atara |
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