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Acetaldehyde synthesis
Beautifull setup! Unfortunate that the experiment wasn't very conclusive.. Please let us know of fut ...
5-9-2009 at 17:32
by: Klute
3-methoxy-4-bromobenzaldehyde
None of your brominating refs are revelant: no where is benzaldehyde brominated. It will not bromina ...
4-9-2009 at 19:23
by: Klute
Isocyanide Synthesis
The procedure I outlined is for preparing N-methyl alkylformamides, from N-alkylformamides.

Inde ...
4-9-2009 at 11:23
by: Klute
Isocyanide Synthesis
I'm sure P2O5 could be used to dehydrate the N-alkylformamides, no? these can be easily made by form ...
4-9-2009 at 01:15
by: Klute
Acetaldehyde synthesis
Please, do post theses pictures!
3-9-2009 at 14:04
by: Klute
Ozonelabs- Synthesis of Raspberry Ketone
Great! I am really pleased someone else tried this out! It's indeed a very fullfilling synthesis!

...
3-9-2009 at 10:36
by: Klute
Kinnear Perren condensation
Interesting reaction, never heard of it before.. What do you plan on doing with the dichloroalkylph ...
3-9-2009 at 10:29
by: Klute
Uses for salicylaldehyde
Anymore info on salicyladoximes? Theses look interesting.. And easy to prepare...
3-9-2009 at 01:02
by: Klute
The short questions thread (2)
hum, doesn't look as simple as I thought.. Too bad..

Totally unrealted question: does anyone see ...
2-9-2009 at 21:16
by: Klute
Preparation of 100% H2SO4
Well it's more the SO3 I worried about, don't want to distill that stuff.. Just addign P2O5 to 98% H ...
2-9-2009 at 07:41
by: Klute
Preparation of 100% H2SO4
Yes, I think that is the most common method, after 100% H2SO4.. But I don't have any anhydrous AlCl ...
2-9-2009 at 07:23
by: Klute
Preparation of 100% H2SO4
Thanks for all the answers.. Looks like much more work that I anticipated.. Like I said I am not r ...
2-9-2009 at 07:10
by: Klute
1-bromo-3,4-methylenedioxybenzene uses
Yes, sesamol looks nice too.
This could even be a way of preparing 2-methoxy-4,5-methylenedioxyben ...
1-9-2009 at 21:19
by: Klute
Preparation of 100% H2SO4
I want to prepare 100% H2SO4 to form alane solution from LiAlH4.. I don't have acces to SO3 or oleu ...
1-9-2009 at 20:55
by: Klute
The short questions thread (2)
Is it possible to C-alkylate benzoquinone? I know addition of various nucleophiles (thiolates, alcol ...
1-9-2009 at 20:04
by: Klute
Smell of Acetaldehyde - What Products?
Just curious, how do you make acetaldehyde? Chromium oxidants? Or a more elaborate method?
1-9-2009 at 18:12
by: Klute
1-bromo-3,4-methylenedioxybenzene uses
Yes, Flic is the word :)
I will contact local university and see if I can get some info on this, or ...
1-9-2009 at 17:49
by: Klute
1-bromo-3,4-methylenedioxybenzene uses
I was kindly given a small amount of 1-bromo-3,4-methylenedioxybenzene, and I'm not sure of what I w ...
1-9-2009 at 12:35
by: Klute
4-alkylthio-2,5-dimethoxybenzaldehyde, Sulfuric Duff reaction
Great! Thanks alot! Definitively on my to-do's list.. Thanks again for sharing all this exceptionnal ...
1-9-2009 at 09:32
by: Klute
N-phenylhydroxylamine..... ?
Did the solution heat up to 60-65°C? Maybe you should activate your zinc before use..
1-9-2009 at 08:26
by: Klute
The taste of salts
I actually tasted sodium nitrite but without putting it in my mouth! :)

When I had that H2S expos ...
1-9-2009 at 07:40
by: Klute
Aspirator/Water outlet for home
I really don't think it worth the hassle of buikding your own aspirator.. it's the kind of thing yo ...
1-9-2009 at 07:24
by: Klute
Fume Cupboard- Ducted or Filtering
Some people should definitively grow up.. Incredible how far some go when behind a damn screen.. Rid ...
31-8-2009 at 16:59
by: Klute
Single molecule, one million times smaller than a grain of sand, pictured for first time
Incredible.

I wonder how they fixed that single molecule of carbon monoxide at the exact point o ...
31-8-2009 at 14:49
by: Klute
N-Mono and N-Di-Alkylation of Phenylalanine?
For the mono-N-alkylation I would suggest the route I used for N-methylphenethylamine, forming the a ...
31-8-2009 at 14:18
by: Klute
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