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Bachelors Degree
Three years ago I was seriously on path to pursuing a bachelor's degree in chemistry. For reasons d ...
3-1-2011 at 19:23
by: ADP
Nitric Acid Synthesis
Explain your method MJP. So you distill at a very high temp and allow lots of NO2 to come over then ...
5-6-2008 at 19:58
by: ADP
Nitric Acid Synthesis
Interesting, I've never heard of someone doing that practically? What is your method of producing NO ...
4-6-2008 at 20:00
by: ADP
Nitric Acid Synthesis
Yes I'm aware of that method:

2NO2 + H2O → HNO2 + HNO3

Not the best for future nitra ...
4-6-2008 at 16:29
by: ADP
Nitric Acid Synthesis
Firstly, I hate to call you on this nodrog19 but what the hell are you trying to do? If you are tryi ...
3-6-2008 at 17:12
by: ADP
Nitric Acid Synthesis
Not for concentrations greater than about 31%...
2-6-2008 at 18:28
by: ADP
stump remover
Spectracide is carried at walmart which I'm pretty sure is 99% KNO3
31-5-2008 at 08:31
by: ADP
Magnetic stirrer/hotplate
Yes all of the applications that I can foresee won't use heat, however I do see how it could be usef ...
31-5-2008 at 08:29
by: ADP
Magnetic stirrer/hotplate
Well here is my new baby, I'll have to just do without the heat, brew

[img]http://img151.imagesha ...
27-5-2008 at 15:31
by: ADP
Nitric Acid Synthesis
I understand your concern, I do believe that someone built a water "recirc" pump to reduce the waste ...
27-5-2008 at 13:24
by: ADP
Nitric Acid Synthesis
The acid mist that does condense in my tube is no problem since I have an aspirator that just leads ...
26-5-2008 at 13:23
by: ADP
Nitric Acid Synthesis
[quote][i]Originally posted by crazyboy[/i]
looks like ADP did it too the thermometer bulb doesn't ...
26-5-2008 at 12:11
by: ADP
Nitric Acid Synthesis
Interesting you mention that problem - texaspete mentioned he had that problem as well, I personally ...
21-5-2008 at 21:46
by: ADP
Glacial Acetic from Vinegar? They did it here
Personally if GAA isn't available in your area, I think the MOST economical route is to purchase sod ...
21-5-2008 at 14:13
by: ADP
Nitric Acid Synthesis
Yeah MJP you're right, I ordered a 10mL Mohr pipet so I'll do that for sure, I might do 50mL or some ...
20-5-2008 at 15:42
by: ADP
Synthesis of Sulfur Trioxide and Oleum: The persulfate method
[quote][i]Originally posted by garage chemist[/i]
In the meantime I have succeeded in making SO3 fr ...
20-5-2008 at 07:53
by: ADP
(HPO3)n Dehydrating agent (polyphosphoric or metaphosphoric acid)
Nice find!
20-5-2008 at 06:13
by: ADP
(HPO3)n Dehydrating agent (polyphosphoric or metaphosphoric acid)
This compound really intrigues me, I wish I still had my 500mL of ACS H3PO4 however I disposed of it ...
19-5-2008 at 21:15
by: ADP
Nitric Acid Synthesis
Thanks, glad you like; I believe my aspirator pulls a vacuum down to at least 30mmHg, but it depends ...
19-5-2008 at 20:21
by: ADP
nitroglycerin
Considering I make the 95%+ nitric from my mixed acids and vacuum distillation, it's not a problem. ...
19-5-2008 at 19:55
by: ADP
nitroglycerin
When it comes to mixed acids I've found that letting the mixed acids react overnight produces a near ...
19-5-2008 at 19:22
by: ADP
cleaning sulfuric acid
I couldn't find rooto at ace but purchased "liquid fire" instead which I know to be good sulfuric. ...
19-5-2008 at 16:42
by: ADP
Magnetic stirrer/hotplate
I personally am looking to buy a magnetic stirrer without the hotplate feature, I've already got one ...
19-5-2008 at 05:10
by: ADP
Glacial Acetic from Vinegar? They did it here
Interesting, now if I could just get a good source of activated carbon. I've done this before but d ...
19-5-2008 at 05:07
by: ADP
cleaning sulfuric acid
Yeah I had a graham condenser that broke once and made me feel the same way. Yeah I'm located in MS ...
19-5-2008 at 04:20
by: ADP
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