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Unexpected product in mucic acid dry distillation
[rquote=682236&tid=159330&author=Lionel Spanner]
This does at least confirm that furoic aci ... |
11-3-2023 at 13:44
by: Alucard |
Separating OTC Xylene
[rquote=669989&tid=158273&author=teodor]
As for sulfonation, I also wanted to try this. Jus ... |
13-1-2022 at 03:30
by: Alucard |
Project: Making thionyl chloride from easy-to-get precursors
[rquote=669212&tid=158187&author=AJKOER]
•NO2 + SO2 -> •NO + SO3 (27)
where th ... |
29-12-2021 at 03:32
by: Alucard |
Project: Making thionyl chloride from easy-to-get precursors
[rquote=669090&tid=158187&author=Monoamine]
Hi Alucard,
I would give it a try. Adding ... |
24-12-2021 at 04:26
by: Alucard |
Project: Making thionyl chloride from easy-to-get precursors
[rquote=668653&tid=158187&author=Monoamine]
The heating mantle was turned to maximum.
A ... |
23-12-2021 at 04:03
by: Alucard |
Can you make p-TSA in situ without too much residual H2SO4?
It is not obligately necessary to use Dean Stark trap when making p-TSA, but I strongly recommend to ... |
6-10-2020 at 01:30
by: Alucard |
ethyl formate - esterification by reactive distillation
[rquote=642365&tid=155432&author=Boffis]and how soluble is water in ethyl formate?[/rquote]
... |
6-8-2020 at 07:35
by: Alucard |
ethyl formate - esterification by reactive distillation
[rquote=642357&tid=155432&author=Fery]Alucard, do not add H2SO4, formic acid is strong enoug ... |
6-8-2020 at 05:52
by: Alucard |
ethyl formate - esterification by reactive distillation
[rquote=636538&tid=155432&author=Fery]
Formic acid is strong enough to catalyze its own e ... |
5-8-2020 at 01:29
by: Alucard |
O-Cresol from Salicylic acid
p-cresol is a bit easier, because it may be derived from p-toluenesulphonic acid, easily made from t ... |
27-12-2019 at 10:30
by: Alucard |
O-Cresol from Salicylic acid
Better policy to obtain o-cresol should be to start from toluene, as well by following route of synt ... |
27-12-2019 at 06:40
by: Alucard |
Synthesis of Sodium Hydroxide (NaOH) via the Caustification Process
The most simple method as I assume is to react Ca(OH)2 with Na2CO3, so :
Na2CO3 + Ca(OH)2 = CaCO3 ... |
1-3-2019 at 02:27
by: Alucard |
Stabilization of diethyl ether by the adition of ethanol
[rquote=603747&tid=145410&author=Tsjerk]
Guess what this ether was made with?
[/rquote] ... |
26-2-2019 at 14:23
by: Alucard |
Stabilization of diethyl ether by the adition of ethanol
[rquote=603723&tid=145410&author=Felab][quote]
I'm pretty sceptical towards your claim this ... |
26-2-2019 at 12:08
by: Alucard |
Stabilization of diethyl ether by the adition of ethanol
[rquote=603621&tid=145410&author=Felab]Since no one seems to give an answer, I will conduct ... |
26-2-2019 at 02:50
by: Alucard |
Selective reduction of nitrotoluenes with Na2S
Today I performed a direct steam distillation of the organic layer gained after second experiment wa ... |
12-2-2019 at 09:46
by: Alucard |
Selective reduction of nitrotoluenes with Na2S
Acquiring for information about densities of a pure chemicals gave following data :
Denisty of :
... |
10-2-2019 at 14:25
by: Alucard |
Selective reduction of nitrotoluenes with Na2S
[rquote=601385&tid=143723&author=S.C. Wack]I'm skeptical that there is some secret Russian m ... |
10-2-2019 at 12:19
by: Alucard |
Selective reduction of nitrotoluenes with Na2S
Today I tried to repeat a Na2S reduction, but with a couple of changes of this process.
To make ... |
10-2-2019 at 09:14
by: Alucard |
Selective reduction of nitrotoluenes with Na2S
[rquote=601178&tid=143723&author=nitro-genes]Do you have the reference for selective reducti ... |
9-2-2019 at 10:00
by: Alucard |
Selective reduction of nitrotoluenes with Na2S
[rquote=601122&tid=143723&author=zed]Seems to me, Toluidine and Acetone might be incompatibl ... |
9-2-2019 at 04:33
by: Alucard |
Selective reduction of nitrotoluenes with Na2S
I've read all the forum topics available prior to reduction of NT's but nothing was found related to ... |
6-2-2019 at 08:46
by: Alucard |
