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2,3-dichloropropene synthesis?
Yea it seems I applied zaitsevs rule to the enolation without thinking to apply it to the isomerizat ...
17-6-2018 at 21:23
by: Assured Fish
2,3-dichloropropene synthesis?
Ok so my target molecule is 2,3-dicholoropropene and i have slightly convoluted way to get there.
I ...
16-6-2018 at 23:44
by: Assured Fish
Alpha halogenation
New thread to go with it too i reckon.



[Edited on 17-6-2018 by Assured Fish]
16-6-2018 at 22:48
by: Assured Fish
Alpha halogenation
Lets turn this thread into something more useful.
I have a question pretaining to enols.

I ask b ...
16-6-2018 at 13:51
by: Assured Fish
Cleaning H2SO4 with H2O2
Caros acid e.g. H2SO5 decomposes at temperatures above 55*C, i do not recall where i read this but i ...
7-6-2018 at 22:07
by: Assured Fish
PhdChemist/Mitigator derail sump
@Mitigator
Please stop trolling like a degenerate moron, you started with a good question about pre ...
24-5-2018 at 16:18
by: Assured Fish
Are there any SM Users in Hawaii?

[quote]
sulfur dioxide smells like rotten eggs
[/quote]
Sulfur dioxide doesnt smell like rotten ...
22-5-2018 at 14:14
by: Assured Fish
Amino ketone formation ( looking for differing opinions on ketonizations
I was actually thinking it would instead polymerize and form black tar, as the heat would be enough ...
17-5-2018 at 22:39
by: Assured Fish
Amino ketone formation ( looking for differing opinions on ketonizations
What i think the OP is attempting to do (judging by his post history), is the following reaction, ba ...
14-5-2018 at 21:41
by: Assured Fish
ChemPlayer the story and the end for now
Wait, i see people have collected all the videos of the larger more mainstream chemistry channel but ...
4-5-2018 at 14:07
by: Assured Fish
Women in Chemistry
Reeboot, you have to remember that cutural factors can over a long enough period of time become impr ...
3-4-2018 at 21:31
by: Assured Fish
Recristallisation of NaBH4
Um it should be noted that sodium borohydride generally reacts with water although im not sure if th ...
19-3-2018 at 00:51
by: Assured Fish
Buying chemicals
Might i ask, what would be so bad about getting a visit from some nice gentlemen in blue.
What Sula ...
11-3-2018 at 22:13
by: Assured Fish
Theoretical Borohydride Production using NaK
Seems I dont see the point, sodium metal melts at 98°c which means it will be a liquid at when heat ...
27-2-2018 at 15:17
by: Assured Fish
Carbamazepine Synthesis
Well they are both the same reaction as far as i can tell.
the first reaction would still require t ...
16-2-2018 at 15:53
by: Assured Fish
Preparation of elemental phosphorus

[quote]
Shouldn't this thread be erased? The DEA lists it. So, how easy is this stuff easy to mak ...
8-2-2018 at 16:28
by: Assured Fish
triphosgene
Triphosgene is made from dimethylcarbonate yes.
CH3OCO2CH3 + 6 Cl2 → CCl3OCO2CCl3 + 6 HCl

But ...
8-2-2018 at 15:19
by: Assured Fish
Carbamazepine Synthesis
There has been a deccent ammount of research done on this compound already, however most routes are ...
7-2-2018 at 20:39
by: Assured Fish
VX hypothetical Thread
Um, im really not sure how well such a topic would go down with the other members here or what exact ...
28-1-2018 at 20:57
by: Assured Fish
Copper chromite wanted to buy..need sent to nz
I have just over 110g however it would take some serious convincing to get me to part with it.

[ ...
25-1-2018 at 20:52
by: Assured Fish
Synthesis of Oxygen Absorbing Crystal (from cobalt)
An interesting material however i dont think equipment is the issue.

http://pubs.rsc.org/en/conte ...
22-1-2018 at 21:00
by: Assured Fish
99% Hbr Gas generation from Hbr Aqueous
Are you asking a question about how to make dry HBr gas?
The way you design you post makes it diffi ...
12-1-2018 at 16:11
by: Assured Fish
DMT synthesis from indole and DMAE
Grignard reagents do not react with tertiary amines.
There is no proton present on the amine for th ...
9-1-2018 at 23:42
by: Assured Fish
Catechol preparation
I would advise strongly against the Dakin reaction, the yields tend to suck balls, also you would fi ...
9-1-2018 at 20:49
by: Assured Fish
DMT synthesis from indole and DMAE
FFS, I know i shouldn't say anything but i cannot help myself.
James Nilep your a degenerate cook a ...
9-1-2018 at 20:23
by: Assured Fish
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