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Substitute for carbon tetrachloride
Carbon tetrachloride can be nearly always be subsitute with Chloroform

If chlorform isn't availab ...
3-1-2019 at 22:55
by: EilOr
Tryptamine Isolation (HELP!!!)
I've had to make nearly one mole tryptamine as an intermediate in ~2010 for my training.
Btw. the ...
3-1-2019 at 22:45
by: EilOr
Thiocyanation of Vanillin using Cu(ii) Advice
Very interesting stuff! Never thought or heard about using thiocyanates that way.

It has to be mo ...
13-6-2018 at 19:08
by: EilOr
Decarboxylation of Glycine to Methylamine?!
[rquote=510766&tid=81256&author=DIBALL]Well in theory it should be possible, or not?

I tr ...
18-3-2018 at 07:46
by: EilOr
Recristallisation of NaBH4
Hi!
I have a few hundred grams of a few years years old NaBH4
It's quality degraded a lot.

I k ...
17-3-2018 at 19:32
by: EilOr
Nitric Acid from Sodium Bisulfite and nitrates
pkA is blablabla, equilibrium is the force you can use!

When I was a 8- or 9yrs old kid and had n ...
6-2-2018 at 11:37
by: EilOr
Ti-(and DABCO) doped alanes as possible catalytic hydrogenation catalysts? (Aka AlH3 from Al and H2 in situ at low pressure)
[rquote=502859&tid=78914&author=Reboot]A lifetime ago, when I was a stupid kid, I tried some ...
6-1-2018 at 21:56
by: EilOr
Ti-(and DABCO) doped alanes as possible catalytic hydrogenation catalysts? (Aka AlH3 from Al and H2 in situ at low pressure)
Nice to hear that someone else is interested in that area :)
It could possibly substitute LAH, BH3* ...
6-1-2018 at 18:40
by: EilOr
Decarboxylation of amino acids (phenylalanine, tryptophan) in various solvents
If smell doesn't bother you - good old genuine terpuntine is OTC a almost perfect solvent for that r ...
5-1-2018 at 13:06
by: EilOr
Synthesis of 2-Nitropropane-1-ol
[rquote=501502&tid=79213&author=Assured Fish]Seems sensible as this same or similar reaction ...
25-12-2017 at 21:15
by: EilOr
Synthesis of 2-Nitropropane-1-ol
Found one myself

Patent: US3560575 A
Preparation of 2-nitro-1-propanol
https://docs.google.com/ ...
25-12-2017 at 00:59
by: EilOr
An Interesting Find on Ebay
For 130$ you could build a 10times better still from steel and Cu parts within one day
24-12-2017 at 00:56
by: EilOr
Synthesis of 2-Nitropropane-1-ol
Hi there!
I wonder if this interesting reactant could be prepared for example from formaldehyde and ...
23-12-2017 at 21:58
by: EilOr
Sticky Foam
Looks like a usual polyurethane to me
https://en.wikipedia.org/wiki/Polyurethane
In my country you ...
23-12-2017 at 19:55
by: EilOr
Silver Nitrate Synthesis
I've done it several times this way with great success, always obtaining a perfectly white sparkling ...
18-12-2017 at 22:11
by: EilOr
Failed attempt at making NO2Cl
[rquote=500836&tid=79069&author=unionised]Could you "dry" the nitric acid with conc sulphuri ...
18-12-2017 at 12:08
by: EilOr
L Lysine hydrochloride to lysine
Lysine*HCl is 1.5kg/l, isoelectric lysine 300g/L so in water should work if you're working in concen ...
17-12-2017 at 05:23
by: EilOr
Looking for diffusion pump oil. Will pay good price.
I think you can use any good high vacuum pump oil, it doesn't has to be a synthetic one
At least in ...
13-12-2017 at 07:06
by: EilOr
40% formaldehyde solution from paraformaldehyde?
[rquote=496681&tid=77411&author=Diachrynic]Does anyone here know if paraformaldehyde is regu ...
13-12-2017 at 02:18
by: EilOr
Ti-(and DABCO) doped alanes as possible catalytic hydrogenation catalysts? (Aka AlH3 from Al and H2 in situ at low pressure)
Hi!
Most likely it's a bullshit idea, as I have no idea about the mechanisms going on, but I like t ...
12-12-2017 at 22:58
by: EilOr

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