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Trinitrotoluene preparation
I am bumping this thread up because I just commenced on my first TNT synthesis. I am doing using the ...
7-7-2025 at 19:10
by: ManyInterests
Shit RDX yields without acetic anhydride
[rquote=701696&tid=161157&author=Microtek]Magnesium nitrate works a lot like sulfuric acid, ...
4-7-2025 at 04:28
by: ManyInterests
Shit RDX yields without acetic anhydride
Understood.

BTW, In terms of the nitric acid. I will be going on a bender making nitric acid agai ...
3-7-2025 at 16:26
by: ManyInterests
Shit RDX yields without acetic anhydride
Yeah, I think I will absolutely need to super dry my AN the next time I use it for anything. I will ...
1-7-2025 at 16:45
by: ManyInterests
Shit RDX yields without acetic anhydride
[rquote=701563&tid=161157&author=Axt]I wouldn't conflate acetic anhydride processes with the ...
28-6-2025 at 16:34
by: ManyInterests
Shit RDX yields without acetic anhydride
[quote]Mix 858g 98% nitric acid and 50g ammonium sulphate and cool to 7C.
Add 70g hexamine in porti ...
27-6-2025 at 22:41
by: ManyInterests
Shit RDX yields without acetic anhydride
Didn't you make a thread similar to this? It's pretty active and recent...
26-6-2025 at 19:03
by: ManyInterests
How to make white fuming nitric acid from red fuming for rdx synthesis
[rquote=701482&tid=161091&author=Microtek]CaCl2 spheres are fine. When I said "preferably fl ...
25-6-2025 at 15:51
by: ManyInterests
How to make white fuming nitric acid from red fuming for rdx synthesis
[rquote=701478&tid=161091&author=Microtek]OK, I am almost certain that the NOx in your nitri ...
24-6-2025 at 23:50
by: ManyInterests
How to make white fuming nitric acid from red fuming for rdx synthesis
[rquote=701461&tid=161091&author=Microtek]It sounds strange to me that you are getting that ...
24-6-2025 at 17:16
by: ManyInterests
How to make white fuming nitric acid from red fuming for rdx synthesis
[quote] Ammoniumnitrate will it work too I bulk orderd 300kg from my supplier from latvia [/quote]
...
24-6-2025 at 11:49
by: ManyInterests
Is my boiling flask OK?
OK, so I learned a lesson with using sodium bisulfate (and what an expensive lesson it is!), especia ...
22-6-2025 at 04:43
by: ManyInterests
How to make white fuming nitric acid from red fuming for rdx synthesis
[rquote=700991&tid=161091&author=Sir_Gawain]Did you rinse the HDN with a little ice cold ace ...
29-5-2025 at 01:51
by: ManyInterests
How to make white fuming nitric acid from red fuming for rdx synthesis
[rquote=700970&tid=161091&author=Sir_Gawain]The hydrogen peroxide method works great for me, ...
28-5-2025 at 14:59
by: ManyInterests
Nickel aminoguanidine diperchlorate
I tested out several detonators using various grades of iNAP that I made, and all worked quite well ...
25-5-2025 at 14:18
by: ManyInterests
Is my boiling flask OK?
OK, I completed the distillation without a hitch. It can still work, but it must be taken VERY serio ...
18-5-2025 at 12:19
by: ManyInterests
Is my boiling flask OK?
[rquote=700803&tid=157398&author=dettoo456]Indeed, way too hot, and the NaHSO4 cake was prob ...
18-5-2025 at 07:59
by: ManyInterests
Is my boiling flask OK?
I decided to bump this up since I had an... interesting situation with a boiling flask.

I was dis ...
18-5-2025 at 06:45
by: ManyInterests
Nuetralizing Ferric Picrate Crystals
[quote] use ethanol or methylated spirits to dissolve them [/quote]

And out of curiosity, once di ...
11-5-2025 at 12:18
by: ManyInterests
Don’t believe chatGPT when it comes to directing groups :)
[rquote=700451&tid=160984&author=Precipitates][rquote=700447&tid=160984&author=Texiu ...
23-4-2025 at 16:00
by: ManyInterests
Substituting nitric acid with ammonium nitrate
Just letting you know, I decided to make some PETN. I got the formula from the thread on PETN that u ...
20-4-2025 at 18:10
by: ManyInterests
Don’t believe chatGPT when it comes to directing groups :)
DO NOT TRUST CHATGPT!

In fact, do not trust ANY AI with chemistry questions. They will get ultra ...
20-4-2025 at 17:56
by: ManyInterests
Picric acid: different instructions
[quote] I need to mention that the new batch used an excess of sodium nitrate. Around 2.5 grams of s ...
22-3-2025 at 11:10
by: ManyInterests
Energetics training classes in PA in June
[rquote=699810&tid=160941&author=Dr.Bob]There used to be a few courses like that, but they h ...
22-3-2025 at 11:02
by: ManyInterests
Accidentally making potassium picrate(?)
I made quite a bit of picric acid in the past (I'm the reason why picric acid is a sticky topic here ...
3-3-2025 at 19:56
by: ManyInterests
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