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Benzyl Iodide/Benzyl Cyanide Synthesis
I have made benzyl chloride from toluene and chlorine using TCCA and hydrochloric acid. The reaction ...
1-10-2014 at 12:21
by: Mercedesbenzene
BF3 + NaBH4 -> BH3 to reduce 3,4 mdns
There is a small different between ethoxy groups and methoxy groups but that is not what will determ ...
17-9-2014 at 11:29
by: Mercedesbenzene
purification of 2,6-dichloropyridine-4-carboxilic acid
Column chromatography would most likely clean it up just fine. The ester might be easier to purify t ...
28-7-2014 at 18:18
by: Mercedesbenzene
Iodine drying
What I do, and it seems to work fairly well, is that I take the wet iodine and put it into a sealed ...
15-3-2014 at 19:42
by: Mercedesbenzene
Source of D-Limonene, OTC?
It is actually fairly easy to get D-limonene OTC. It is sold as an citrus based ski wax remover or s ...
4-3-2014 at 21:29
by: Mercedesbenzene
Please can any one help me on epichlorohydrin production method
Im going to say cost. Bleach and lye are much cheaper than mCPBA
16-8-2013 at 18:06
by: Mercedesbenzene
Potassium nitrate from 15-15-15 fertilizer
You should try to confirm that the fertilizer does actually have nitrates in it. From what I have fo ...
8-8-2013 at 07:14
by: Mercedesbenzene
Epoxide reduction
I didn't find any papers on what you are trying to do, but by looking at it I can make a hypothesis ...
2-8-2013 at 12:02
by: Mercedesbenzene
Organic Chlorinations?
Benzyl alcohol can quite simply be made from an Sn2 reaction of benzyl chloride with some kind of hy ...
22-7-2013 at 16:17
by: Mercedesbenzene
Organic Chlorinations?
I personally liked the radical chlorination of toluene. It chlorinates the methyl group to yield the ...
21-7-2013 at 21:31
by: Mercedesbenzene
Interest in carbon disulfide?
Where abouts are you located? I might be interested in a small quantity, say 20-50mL. Only if you ar ...
6-7-2013 at 13:42
by: Mercedesbenzene
Question regarding stability of carbocations...
for I and III its quite simple, I is just a random carbocation but III is anti aromatic, 4n=4.

so ...
28-6-2013 at 07:25
by: Mercedesbenzene
Thermometer Well for Nitric Acid
The average thermometer is around 5-8mm in diameter I think. Best way is to measure your thermometer ...
13-6-2013 at 06:40
by: Mercedesbenzene
Thermometer Well for Nitric Acid
Buy some fluoropolymer O-rings! They are super cheap from here.

http://www.mcmaster.com/#o-rings/ ...
10-6-2013 at 20:52
by: Mercedesbenzene
Cooling bath at -10*C
Well actually sodium chloride in water solutions can effectively be cooled to around -17 C without f ...
2-6-2013 at 20:04
by: Mercedesbenzene
Scared to ask science teacher about doing chemistry in school lab
I asked my chemistry teacher this exact question in high school. The next week I was in the lab doin ...
30-5-2013 at 20:59
by: Mercedesbenzene
Looking for advice on oxygen analzyers
Hello everyone. I am looking to find a digital oxygen analyzer for a glovebox that I am currently wo ...
23-5-2013 at 20:19
by: Mercedesbenzene
Nitric Acid, specific questions from a newbie
A way to clean out the acids left over assuming you don't want to keep them for any reason is to fil ...
20-5-2013 at 22:00
by: Mercedesbenzene
distilled from molecular sieve?
Usually molecular sieves hold water up until 175-200 C. If your solvent boils much lower than that i ...
1-5-2013 at 16:49
by: Mercedesbenzene
amateur cannula sources?
I had this problem as well but I found a great solution for it. Go to amazon or ebay and buy some st ...
1-5-2013 at 16:34
by: Mercedesbenzene
Know of any common industrial cleaning chemicals worth having?
http://householdproducts.nlm.nih.gov/index.htm
Under ingredients you can find chemicals that are in ...
3-4-2013 at 07:46
by: Mercedesbenzene
Looking for a Source of n-butyllithium
I can't remember off the top of my head who wrote the paper, but yes, it's Li metal and bromobutane. ...
29-3-2013 at 14:50
by: Mercedesbenzene
Looking for a Source of n-butyllithium
I have been looking for a source of n-butyllithium for quite some time now without much luck. I have ...
28-3-2013 at 13:57
by: Mercedesbenzene
Dry Ice
Not sure if you live near a university, but in many molecular biology labs they have many of the sup ...
26-3-2013 at 07:54
by: Mercedesbenzene
p-toluenesulfonic acid synthesise problem
p-toluenesulfonic acid is highly soluble in water. What you need to do and the procedure I have used ...
25-3-2013 at 15:41
by: Mercedesbenzene
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