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Potassium Peroxodisulfate with 50% Sulfuric Acid Distillation - First Success
Hello,
As stated in my last post, I tried to electrolytically generate some Sodium Perborate. I t ... |
6-12-2025 at 19:29
by: Mister Double U |
H2O2 By Electrolysis
An interesting read!
With a well-designed cooling system, it could be a route.
I have also thoug ... |
10-9-2025 at 17:34
by: Mister Double U |
H2O2 By Electrolysis
I apologize for being grouchy, chempyre235.
It's probably my frustration that I have not made bett ... |
8-9-2025 at 14:30
by: Mister Double U |
H2O2 By Electrolysis
chempyre235,
You convinced me, it seems that Phthalic Anhydride can be made by the amateur.
In g ... |
8-9-2025 at 11:03
by: Mister Double U |
Experiment with Phosphate Addition - Small Success
Hello,
As mentioned, I also wanted to conduct a run and see which effect PO4[3-] has on the whole ... |
7-9-2025 at 06:04
by: Mister Double U |
Powerful ozonizer, is it possible at home?
Hello DennyDevHE77,
Many years ago, I built an Ozone generator.
It used a neon sign transformer ... |
6-9-2025 at 09:31
by: Mister Double U |
H2O2 By Electrolysis
Here some suggestions ChatGPT-5 gave for the process:
Key Hydrolysis Conditions (from US Pate ... |
6-9-2025 at 05:06
by: Mister Double U |
H2O2 By Electrolysis
Here the result of the last distillation attempt - failure:
Before I started distillation, I heat ... |
6-9-2025 at 04:58
by: Mister Double U |
H2O2 By Electrolysis
Hello chempyre235,
I am not sure how easy it would be to make the Phthalocyanine.
As you stated, ... |
6-9-2025 at 04:39
by: Mister Double U |
H2O2 By Electrolysis
Here the results for the Persulfate content of the NaHSO4 electrolysis:
[file]107220[/file]
2.47 ... |
4-9-2025 at 15:42
by: Mister Double U |
H2O2 By Electrolysis
Just tested the second ammonium persulfate solution. Please note that this is not the distilled H2O2 ... |
1-9-2025 at 16:46
by: Mister Double U |
H2O2 By Electrolysis
@Radiums Lab,
I see where you are going with the Pt.
On the other hand, it would be nice to have ... |
31-8-2025 at 17:10
by: Mister Double U |
H2O2 By Electrolysis
@Radiums Lab,
I heard that Sodium can be burned in excess Oxygen to yield Sodium Peroxide.
Doing ... |
31-8-2025 at 12:23
by: Mister Double U |
Failure Again
Just tested the distillate by the usual copper wire and boiling method.
No gas evolution was observ ... |
30-8-2025 at 20:19
by: Mister Double U |
H2O2 by Ammonium Persulfate Hydrolysis & Vacuum Distillation
Hello Folks,
As promised, I finished electrolyzing the NH4HSO4 solution. And it is currently dist ... |
30-8-2025 at 17:06
by: Mister Double U |
H2O2 By Electrolysis
clearly_not_atara,
Currently distilling some H2SO4 to make a fresh batch of NH4HSO4 through Urea ... |
24-8-2025 at 02:09
by: Mister Double U |
H2O2 By Electrolysis
Alkoholvergiftung,
I heard that Ammonium Persulfate is presumably easier to create than the other ... |
23-8-2025 at 09:54
by: Mister Double U |
Distillation of a purchased 3% Hydrogen Peroxide Solution
After the previous failures, I wanted to see, if H2O2 can be distilled at 100mbar without decomposit ... |
23-8-2025 at 09:42
by: Mister Double U |
Distillation of K2S2O8 with 30% H2SO4 - Failure
Attempted the distillation of ~70g Potassium Persulfate with ~200ml 30% H2SO4 with my new vacuum pum ... |
23-8-2025 at 09:32
by: Mister Double U |
Potassium Peroxodisulfate
Hello,
Last week I decided to prepare some K2S2O8. I am not sure if it will be a good precursor t ... |
22-8-2025 at 16:49
by: Mister Double U |
H2O2 By Electrolysis
Thanks for the info, bariumbromate!
I am looking forward to trying it out then :-) |
18-8-2025 at 14:30
by: Mister Double U |
H2O2 By Electrolysis
MrDoctor,
I was thinking about bleeding some air into the system to have the air carry H2O/H2O2 o ... |
18-8-2025 at 01:13
by: Mister Double U |
Persulfuric Acid
Hello,
I thought about the problem of generating H2O2 by electrolysis of Sulfates, and I think it ... |
17-8-2025 at 12:06
by: Mister Double U |
Vacuum
Hello 4-Stroke,
Have you thought about using a vacuum pump at the end of your condenser.
That wa ... |
29-6-2025 at 02:12
by: Mister Double U |
H2O2 By Electrolysis
Thank you, Belowzero!
I think with my current equipment I am almost at an end point here.
One mo ... |
23-6-2025 at 16:39
by: Mister Double U |
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