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Discrepancies in Shulgin's Synthesis? Tryptamine + MeI = 1-Me-TMT?
DrMethyl, I'm not sure if I'm following you. The goal is to [i]avoid[/i] methylation of the indole n ... |
25-11-2015 at 17:13
by: Quatro |
Alternative methylation reagents to form quat tryptamine salts?
Well what I was trying to say is, in the absence of a base an 88% - 99% yield should be accomplished ... |
25-11-2015 at 12:55
by: Quatro |
Alternative methylation reagents to form quat tryptamine salts?
I completely understand where you're coming from JJay, I respect your opinion.
The synthesis of t ... |
25-11-2015 at 07:43
by: Quatro |
Alternative methylation reagents to form quat tryptamine salts?
JJay, this is Nicodem's quote from a different thread
[rquote=211948&tid=16425&author=Nic ... |
23-11-2015 at 11:02
by: Quatro |
Alternative methylation reagents to form quat tryptamine salts?
I had this same discussion with my friend Crowfjord. Although maybe Hunig's base could be used, stro ... |
22-11-2015 at 16:40
by: Quatro |
Alternative methylation reagents to form quat tryptamine salts?
Well I think the low yield probably has to do with the positively charged amine hydroiodides that fo ... |
22-11-2015 at 15:42
by: Quatro |
Alternative methylation reagents to form quat tryptamine salts?
Thanks for the info. Where are you getting those numbers that 50°C is necessary for MeI to react at ... |
22-11-2015 at 12:01
by: Quatro |
Alternative methylation reagents to form quat tryptamine salts?
Thanks Nicodem
In an old thread you mentioned how only MeCl is significantly less electrophilic t ... |
22-11-2015 at 06:24
by: Quatro |
Recommendations for decent rotovap
I think that rotovap is just another word for reduced pressure distillation...
I've also looked o ... |
21-11-2015 at 20:35
by: Quatro |
Alternative methylation reagents to form quat tryptamine salts?
Well you could reflux H3PO4, NaI, and MeOH to do it, but that's besides the point. I was wondering i ... |
12-11-2015 at 07:57
by: Quatro |
Preparation of Iodomethane
Does anyone have experience making MeI by gassing a saturated solution of KI in MeOH with HCL gas?
... |
10-11-2015 at 20:58
by: Quatro |
L-tryptophan decarboxylation
Well yes, the Rotovap would be used to remove the acetophenone from the tryptamine/acetophenone mixt ... |
9-11-2015 at 11:30
by: Quatro |
L-tryptophan decarboxylation
Why would vacuum fractionation be better than plain vacuum distillation? I understand fractional dis ... |
8-11-2015 at 19:46
by: Quatro |
L-tryptophan decarboxylation
Oh wow, you would think Wikipedia would list the boiling point at standard atmospheric pressure, but ... |
7-11-2015 at 11:13
by: Quatro |
Acetophenone
I feel like there should be a simple solution to isolating Tryptamine from the Acetophenone mixture. ... |
7-11-2015 at 08:33
by: Quatro |
Local Chemical suppliers
I think the fact that you live in India explains the cheap chemical prices. (And probably larger ava ... |
4-11-2015 at 17:07
by: Quatro |
New chemicals for sale !
Well it did seem suspicious. Some of the prices are ridiculously cheap like a liter of acetone for o ... |
3-11-2015 at 09:59
by: Quatro |
New chemicals for sale !
Oh this is interesting. A user who registered on the same day that he posts the review for the chemi ... |
2-11-2015 at 16:06
by: Quatro |
Discrepancies in Shulgin's Synthesis? Tryptamine + MeI = 1-Me-TMT?
After filtering the solids from the solution, Shulgin gets a mixture of Tryptamine, NMT, DMT, and TM ... |
1-11-2015 at 12:45
by: Quatro |
Discrepancies in Shulgin's Synthesis? Tryptamine + MeI = 1-Me-TMT?
Very elegantly put Crowfjord! That makes sense... A sterically hindered base might not be advantageo ... |
1-11-2015 at 10:53
by: Quatro |
Discrepancies in Shulgin's Synthesis? Tryptamine + MeI = 1-Me-TMT?
Ahhh thank you very much for the explanation! I should have noticed their use of NaOH...
If you w ... |
1-11-2015 at 10:25
by: Quatro |
Discrepancies in Shulgin's Synthesis? Tryptamine + MeI = 1-Me-TMT?
Alkylating tryptamine with a methyl halide will produce a tetraalkylammonium product.
[url=https: ... |
1-11-2015 at 07:28
by: Quatro |
