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double bond reduction of alpha-methylnitrostyrenes with NaBH4
My ref is my empirical data ;)
Btw. I've had higher, nearly quanititative yields on similar substra ...
27-9-2014 at 13:47
by: Rabodon
the hunt for the reducing agent
[rquote=348819&tid=34833&author=bbartlog]What procedure are you trying to execute? There are ...
27-9-2014 at 11:11
by: Rabodon
the hunt for the reducing agent
[rquote=348341&tid=34833&author=Rabodon]My fav to Reduce NO2-Groups is Zn/HCOOH in EtOH.
Yo ...
27-9-2014 at 10:57
by: Rabodon
the hunt for the reducing agent
Has anyone here had success using HCOOH + ammonium formiate or potassium formiate + Pd/C for any red ...
27-9-2014 at 05:25
by: Rabodon
double bond reduction of alpha-methylnitrostyrenes with NaBH4
[rquote=347578&tid=5436&author=Templar]Wasn't there something about requiring several molar ...
25-9-2014 at 18:14
by: Rabodon
the hunt for the reducing agent
My fav to Reduce NO2-Groups is Zn/HCOOH in EtOH.
You can make a slurry of fine Zn powder (you can a ...
25-9-2014 at 17:59
by: Rabodon
L-tryptophan decarboxylation
Why all this fuzz about Tryptophane decarboxylation?

I've done it once in terpentuine (genuine st ...
17-9-2014 at 17:12
by: Rabodon
Report on Decarboxylation of Tryptophan in various solvents
Thank you for sharing your notes!

I got also quite high yields, at least 80% after workup/purific ...
6-7-2014 at 16:14
by: Rabodon
Lithium metal from LiPo (Notebook) batteries?
Thank you for your answers!
I've googled around a lot and found that 18650 cells do contain LiMn2O ...
18-6-2014 at 12:18
by: Rabodon
Lithium metal from LiPo (Notebook) batteries?
Hi!
I have ton's of LiPo cells (18650 type, 3,7V 2600mAh) from notebook batteries lying around. ht ...
16-6-2014 at 10:08
by: Rabodon

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