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How fast do benzylic chlorides hydrolyze in cold water?
I know the reaction occurs, but I am not sure to what extent.
I'm working on a polymeric macromo ... |
5-2-2016 at 12:56
by: RareEarth |
Magnetic Stirrer suddenly stopped working, advice?
Well I took it apart, and undid like 10 different connectors to realize there was nothing wrong insi ... |
24-1-2016 at 16:07
by: RareEarth |
Magnetic Stirrer suddenly stopped working, advice?
I guess I'll take it apart, since I don't have couple hundred bucks to spend on a new plate. Fortuna ... |
24-1-2016 at 14:22
by: RareEarth |
Magnetic Stirrer suddenly stopped working, advice?
It was just in refluxing water, and I tried 4 other stir bars. I believe the issue is mechanical, ma ... |
24-1-2016 at 01:04
by: RareEarth |
Magnetic Stirrer suddenly stopped working, advice?
Last night when I was stirring something, the stir bar suddenly started spazzing out flying all over ... |
23-1-2016 at 22:50
by: RareEarth |
Acylation of alcohol with acyl chloride - effect on chirality?
Ah, you guys are right. I had a brain fart moment there. My brain seemed to be mixing up information ... |
15-1-2016 at 18:04
by: RareEarth |
Acylation of alcohol with acyl chloride - effect on chirality?
I was having a little difficulty finding information on this. If an acyl chloride is reacted with a ... |
15-1-2016 at 17:17
by: RareEarth |
Heating mantle turning yellow/red upon heating?
I thought most mantles couldn't get physically hotter than 450f?
I do have a temp controller but ... |
5-1-2016 at 16:50
by: RareEarth |
Heating mantle turning yellow/red upon heating?
I haven't used a heating mantle in a while, but I found one in storage. When I went to test it by bo ... |
5-1-2016 at 13:47
by: RareEarth |
Alkylation of PVC by Iodide salt catalysis?
Here are some links of relevence. The fineklstein reaction to form the polyvinyl iodide does indeed ... |
29-10-2015 at 14:32
by: RareEarth |
Alkylation of PVC by Iodide salt catalysis?
I could easily get the PVC to dissolve, and I could throw in an iodide-based quaternary salt to over ... |
28-10-2015 at 10:51
by: RareEarth |
Synthesis of 4-Nitroaniline (Video) Why did it catch fire?
You have an awesome camera. Good video editing as well. Can I ask what kind of camera you use?
Do ... |
27-10-2015 at 16:34
by: RareEarth |
OTC Calcium Hydroxide
I don't see anything wrong. To ensure maximum conversion of the NaOH, it wouldn't hurt to use excess ... |
27-10-2015 at 15:30
by: RareEarth |
OTC Calcium Hydroxide
[rquote=425009&tid=64128&author=JJay]Calcium hydroxide is 100x as soluble in water as calciu ... |
27-10-2015 at 14:30
by: RareEarth |
OTC Calcium Hydroxide
Calcium Salts usually have very poor solubility in water, in my experience. According to wikipedia t ... |
27-10-2015 at 13:48
by: RareEarth |
Filtering
Unless you have it below its melting point at -34 degrees, then yes I would think that as a liquid, ... |
27-10-2015 at 13:41
by: RareEarth |
Alkylation of PVC by Iodide salt catalysis?
Could it be plausible to dissolve PVC (the polymer), and then use an iodide salt to cause an in-situ ... |
27-10-2015 at 13:07
by: RareEarth |
Inefficient/Bad Hot Plate?
[rquote=424911&tid=64104&author=zombiedude1]
Either way, I'm starting to think these hotp ... |
27-10-2015 at 10:28
by: RareEarth |
Good Vacuum Distillation Experiment
DCM from paintstripper is a good suggestion. DCM is pretty valuable for extracting organics, and oft ... |
25-10-2015 at 19:24
by: RareEarth |
Inefficient/Bad Hot Plate?
I've noticed my hotplate seems to be quite weak lately. At first I thought it was all in my head.... ... |
25-10-2015 at 19:15
by: RareEarth |
Technical obstacles in creating your own vacuum pump from a positive displace pump?
There's a lot of different positive displacement pumps on the market. Even some new "silent" externa ... |
25-10-2015 at 19:11
by: RareEarth |
Small manual dispenser pump for small containers?
I used to have a plunger type pump, but really I spilled more with that thing than if I just poured ... |
23-10-2015 at 19:11
by: RareEarth |
Small manual dispenser pump for small containers?
I'm looking for something that will make it easier to transfer liquids from 1-gallon containers to s ... |
23-10-2015 at 18:38
by: RareEarth |
Chloroacetyl Chloride - Lachrymator, how much so?
Luckily the product I am reacting it with is an insoluble support so I can't imagine much to go wron ... |
22-10-2015 at 18:32
by: RareEarth |
Chloroacetyl Chloride - Lachrymator, how much so?
I don't presently have a fume hood, but ventilation yes. I wasn't planning to heat it or anything, d ... |
22-10-2015 at 18:09
by: RareEarth |
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