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1,4-Dioxane from Ethylene Glycol and H2SO4
Interesting update. I finally got around to cleaning up all the different fractions I collected from ... |
5-3-2023 at 16:13
by: TLutman |
my rogue 40/35 ground glass joint
You can go to most auto parts stores and get lapping compound. There is fine and course grit, and it ... |
21-1-2023 at 19:10
by: TLutman |
1,4-Dioxane from Ethylene Glycol and H2SO4
I have about 500ml of distilled H₂SO₄ left and a couple liters of liquid fire drain cleaner. I a ... |
17-11-2022 at 14:54
by: TLutman |
1,4-Dioxane from Ethylene Glycol and H2SO4
I added more koh earlier, and it went from red to black. All koh dissolved, but the returns on the e ... |
16-11-2022 at 19:19
by: TLutman |
1,4-Dioxane from Ethylene Glycol and H2SO4
After some additional digging I found this is formulated for gas and Diesel engines. It has a few mo ... |
16-11-2022 at 15:52
by: TLutman |
Protecting vacuum from H2SO4 vapors?
That is what I did. Pick your vactubing wisely. I had 3/8” clear and the heat tends to soften it, ... |
15-11-2022 at 14:57
by: TLutman |
1,4-Dioxane from Ethylene Glycol and H2SO4
It may very well be this antifreeze brand.
Distilling the E.G. from the antifreeze left varying am ... |
14-11-2022 at 19:42
by: TLutman |
1,4-Dioxane from Ethylene Glycol and H2SO4
After little hiatus with other projects, I’m back to this
I tried running the same antifreeze t ... |
14-11-2022 at 15:39
by: TLutman |
Purification of drain-cleaner acid
You need to remember what the acid is for, namely unclogging plugged plumbing. They contain corrosio ... |
26-1-2022 at 17:39
by: TLutman |
Hello and help for lightsensitive paint
Have you tried pre sensitized boards? That’s what I’ve always used with decent results, even wit ... |
28-12-2021 at 18:24
by: TLutman |
Introduction/Suggestions
I live in the Midwest as well, but as you know, that’s a whole lot of territory. Narrow it down a ... |
28-12-2021 at 18:10
by: TLutman |
Curious about HS result
Performed your test this morning. The Compound readily dissolved in a weak NaOH solution with no res ... |
31-5-2021 at 04:59
by: TLutman |
Curious about HS result
Watched chemplayer, dougs lab, Nile red and NurdRage videos on hydrazine sulfate and wanted to give ... |
30-5-2021 at 06:59
by: TLutman |
1,4-Dioxane from Ethylene Glycol and H2SO4
Tried this again, paying mind to what was said.
First thing, it wasn’t Traveller brand, it is Pri ... |
3-5-2021 at 18:21
by: TLutman |
1,4-Dioxane from Ethylene Glycol and H2SO4
[rquote=658666&tid=157330&author=clearly_not_atara]Sounds like it worked out. 
The othe ... |
22-4-2021 at 13:30
by: TLutman |
1,4-Dioxane from Ethylene Glycol and H2SO4
I have the dioxane stirring now with NaOH. It’s looking good so far, with only some clumping of th ... |
21-4-2021 at 17:14
by: TLutman |
1,4-Dioxane from Ethylene Glycol and H2SO4
Label calls ethylene glycol, diethylene glycol, water, mixed corrosion inhibitors.
As for the hi ... |
21-4-2021 at 16:23
by: TLutman |
Dioxane didn’t end well
I was going through NurdRage vids and decided to do the dioxane from antifreeze synthesis . I used T ... |
21-4-2021 at 14:06
by: TLutman |
NH₃
I originally tried on a small scale using a Pyrex washing bottle. It didn’t appear to have enough ... |
21-8-2020 at 16:00
by: TLutman |
NH₃
The urea / NaOH never foamed a bit. Vapors burned the cuts/ abrasions I always seem to have, and bei ... |
20-8-2020 at 18:41
by: TLutman |
NH₃
I’m about as noob as it gets, trying to not make things that easily can get out of hand until I ge ... |
20-8-2020 at 16:36
by: TLutman |
Suggestions for glass joint-grease that won't get stuck after vacuum distillations?
I’ve been using dielectric silicone grease with no issues. It’s readily available from most car ... |
6-8-2020 at 14:50
by: TLutman |
Distillation Ideas
I’m curious what substance has a bp close enough to sulfuric acid to necessitate fractional distil ... |
6-8-2020 at 14:20
by: TLutman |
Acid problems
Heating too fast? I thought I was being conservative on it, but I will try slowing it down a bit. I ... |
10-7-2020 at 18:33
by: TLutman |
Acid problems
Just looking for some opinions on what happened with a couple distillations of acid.
First was li ... |
10-7-2020 at 15:01
by: TLutman |
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