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Experimental: Alternative to Al/Hg - the Al/Cu
[rquote=344982&tid=30297&author=the gay doctor2]Hello, I have been watching this thread with ... |
25-10-2014 at 05:56
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
Templar : Did you try a regular Al/Hg on the styrene?
If a regular Al/Hg doesnt work then odds ar ... |
18-8-2014 at 03:56
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
@crystal
No attempt with Ga-salts yet, only Ga metal and it works pretty good. See http://www.scien ... |
16-8-2014 at 15:33
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
NaBH4 was never used, so it should perform without it.
BTW what was the result of the steam disti ... |
11-8-2014 at 08:45
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Ga
Generally Ga alone should give the same results you are seeing, assuming your amalgam actually shows ... |
21-7-2014 at 21:28
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Ga
I take it your Ga is very pure. Usually with recycled Ga combined with Al it will react pretty fast ... |
21-7-2014 at 07:46
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Ga
Hm, it was tried to use less gallium at some points but this produced some kind of super-reactive dr ... |
29-6-2014 at 17:07
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Ga
@Burner
Indeed, the amalgam is not liquid, but some mixture between liquid and solid.
@Crypto
... |
29-6-2014 at 15:29
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Ga
[b]References[/b]
There has been plenty of talks about using gallium to activate Al, both on this f ... |
29-6-2014 at 12:51
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
How much Ga did you use in place of mercury? Usually less than a gram mercury salt is used. Did you ... |
29-6-2014 at 10:40
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
Working on some gallium experiments now actually.
Gallium is awesome in that it allows complete c ... |
29-6-2014 at 09:53
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
Hm, did you check the PH of the steam distillate? |
23-6-2014 at 09:45
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
Did you separate the other product from the steam distillate first, before you re-extracted it again ... |
23-6-2014 at 06:39
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
Benzyl chlorides main effect should be a massive amount of tears in your eyes. If you smell it, you ... |
22-6-2014 at 22:16
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
Use only CuCl2...no NaCl is neccessary.
So only 1-2g CuCl2. |
21-6-2014 at 06:09
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
Interesting, well, it's definitely not the denat EtOH.
PEA has been tried before and this has ne ... |
21-6-2014 at 04:24
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
Chloroform? Hmm, that's weird. What exactly is the substrate you are reducing?
If you have access ... |
21-6-2014 at 02:06
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
10g copper chloride and 20g table salt? Damn. That is a lot! Notice in the two posts that was made a ... |
20-6-2014 at 18:00
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
Some of the copper sulphate is prepared from H2SO4 and can have a very acidic effect. So best is pro ... |
16-6-2014 at 19:01
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
Yeah, there has sometimes been observed particles hanging around in the interface between organic/in ... |
15-6-2014 at 13:19
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
A little update, this reaction was ran again with 10x scale, and this time it was used only 5g CuCl2 ... |
12-6-2014 at 18:27
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
@Crowfjord Steam distill it internally. Just add a bunch of water and heat it, re-add water occasion ... |
7-6-2014 at 10:44
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
[rquote=332873&tid=30297&author=polsaer]To good to be true, but i gave it a run.
2,5 gr Al
... |
3-6-2014 at 11:05
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
[rquote=331267&tid=30297&author=madscientist]
Have you tried running this reaction in neutr ... |
19-5-2014 at 01:05
by: TheCopperMan |
Experimental: Alternative to Al/Hg - the Al/Cu
A little update, the same exact reaction was ran as in the original post, but this time using 1.5g C ... |
12-5-2014 at 16:20
by: TheCopperMan |
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