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Workup is degrading chemical?
So I've done this reaction several times to produce the chemical Emylcamate:
Trifluoroacetic acid ... |
11-8-2018 at 00:57
by: Xylitol |
Grignard work up
[quote]
The washing step doesn't need a specific amount of sulfuric acid because the alkoxide wi ... |
17-10-2016 at 23:39
by: Xylitol |
Grignard work up
I also forgot to mention: How to I test the PH of the ether or do I need to separate it first and ch ... |
16-10-2016 at 20:00
by: Xylitol |
Grignard work up
I completed the reaction last week and here are the results:
After oven drying the glassware and ... |
16-10-2016 at 19:47
by: Xylitol |
Grignard work up
Thanks for the reply. The only two acids I have in my lab now are HCl and sulfuric. Do you think it' ... |
1-10-2016 at 01:43
by: Xylitol |
Grignard work up
I am going to be doing a grignard reaction for the first time (and I'm a novice).
I am planning o ... |
30-9-2016 at 17:08
by: Xylitol |
Cyclopropyl grignard
Thanks for the help. Is that reference specific to this reaction or is it just general info? I want ... |
5-9-2016 at 09:56
by: Xylitol |
Cyclopropyl grignard
[quote]
If you do already have it though, yes, it will probably be very difficult to work with as ... |
4-9-2016 at 14:25
by: Xylitol |
Cyclopropyl grignard
I want to synthesize the chemical: 2-cyclopropyl-2-butanol
I have never done a grignard reaction ... |
4-9-2016 at 13:17
by: Xylitol |
Alkylation of terminal alkyne on alcohol
If I have a tertiary acetylenic alcohol and I want to attach an alkyl group to the end of the termin ... |
3-6-2016 at 23:35
by: Xylitol |
Removing/neutralizing TFA from carbamate
[rquote=443625&tid=65742&author=Metacelsus]Maybe you could try adding solid anhydrous potass ... |
29-3-2016 at 11:38
by: Xylitol |
Removing/neutralizing TFA from carbamate
Let me start off by saying I'm a beginner and maybe missing something obvious.
I have synthesized ... |
28-3-2016 at 15:31
by: Xylitol |
What is the risk of ordering this?
I want to purchase a chemical that is not restricted or listed anywhere, but can be used as a precur ... |
22-3-2016 at 22:34
by: Xylitol |
Carbamate Synthesis
I performed the reaction and boiled off/evaporated as much solvent as possible. The resulting liquid ... |
25-10-2015 at 21:12
by: Xylitol |
Carbamate Synthesis
I am also interested in this synthesis, but I am a beginner and I'd like some clarification before p ... |
8-10-2015 at 06:07
by: Xylitol |
