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Acid-catalysed halogenation
I would only start with like a drop or two of strong acid catalyst. It should be all that's necessar ...
27-7-2006 at 15:02
by: a123x
Methylation with MeNO3
Seeing as methyl nitrate is somewhat easier to prepare compared to MeI and DMS, I was considering at ...
25-6-2006 at 17:03
by: a123x
the most beautiful residue
Idk, I think I may have found some crystal residue which is even more beautiful, or at least rivals ...
1-6-2006 at 10:55
by: a123x
Zinc reduction for 2C-H from nitrostyrene
I was trying to figure out an alternative work-up for this synthesis and this is what I thought of:
...
16-3-2006 at 21:32
by: a123x
Uses of Arenes
Solvents
Adhesives
Pesticides
Flavorings
Scents
Pharmaceuticals
Polymers
Explosives
Ph Indic ...
5-2-2006 at 18:43
by: a123x
Uses of Arenes
Are you sure you read something about arenes? Are you sure it wasn't nothing?

Arene is another te ...
30-1-2006 at 16:08
by: a123x
Improvised Vacuum Filtration
The following is method of improvised vacuum filtration which I've used a number of times. It isn't ...
12-1-2006 at 21:01
by: a123x
Zinc reduction for 2C-H from nitrostyrene
I successfully made 4-methoxyphenethylamine(or at least I think I did). I reacted 1g of anisaldehyde ...
12-1-2006 at 15:10
by: a123x
Elemental sodium from engine valves...
My uncle works in a high performance automotive shop and had several such valves. He gave me a few o ...
9-1-2006 at 22:23
by: a123x
Zinc reduction for 2C-H from nitrostyrene
Is this method only applicable for making 2C-H or will it work for reducing a variety of nitrostyren ...
4-1-2006 at 00:46
by: a123x
Reaction of amine and bromine water
The amine group is very strongly activating to the aromatic ring in aniline. The bromine adds itself ...
2-1-2006 at 01:49
by: a123x
Ethyl Iodide
[quote][i]Originally posted by hinz[/i]
Chochu3 the last reaction you mentioned won't work eighter. ...
18-12-2005 at 22:17
by: a123x
Methods of adding OH/CH3O
I'm sure that a Sandmeyer reaction in water will convert quite readily to the hydroxy compound ...
21-11-2005 at 01:24
by: a123x
Methods of adding OH/CH3O
In making things like 5-hydroxyvanillin, 3,4,5-trimethoxybenzaldehyde, and other compounds, it' ...
20-11-2005 at 19:51
by: a123x
Strange Reaction and possible accidental Indicator
I don't recall all the details of the bromination(it was over a couple months ago). The acid wa ...
22-10-2005 at 20:28
by: a123x
Strange Reaction and possible accidental Indicator
So, a while ago I tried brominating anisaldehyde with a brominating solution made by reaction NaBr w ...
22-10-2005 at 14:26
by: a123x
New Energetic Materials - Current Research
[quote][i]Originally posted by Quince[/i]
Some things are not clear from the article. For example, ...
5-9-2005 at 13:21
by: a123x
Beautiful! Al + Br2
I've recently been experimenting with making alkoxides by the electrolysis of solutions of NaBr ...
19-6-2005 at 20:32
by: a123x
3,4,5-trimethoxy-beta-nitrostyrene synthesis
I thought of another possible route to making 3,4,5-trimethoxybenzaldehyde, starting with anisaldehy ...
19-6-2005 at 14:46
by: a123x
Sodium methoxyde by electrolysis?
I was actually thinking along the lines of making the sodium amalgam in a methanol solution and then ...
11-6-2005 at 22:06
by: a123x
question about ethanol synthesis
An idea I had for making rather pure ethanol was to simply take ethyl acetate and react it with NaOH ...
8-6-2005 at 21:30
by: a123x
Sodium Ethoxide and anhydrous EtOH
[quote][i]Originally posted by Tacho[/i]
I am currently trying to turn a bromo benzaldehyde into a ...
8-6-2005 at 20:10
by: a123x
Naphthol anologs of TNP
Well, I've lately been looking into the bromination of aromatic rings for the purpose of then r ...
3-6-2005 at 16:47
by: a123x
Sodium methoxyde by electrolysis?
Sodium amalgam to make sodium methoxide. I recently read that sodium amalgam can be produced by elec ...
31-5-2005 at 21:42
by: a123x
Theoretical Synthesis of 3,4,5-Alkoxy-PEA
So far I've been having a fairly good time of decarboxylating the tyrosine by refluxing it in a ...
6-5-2005 at 11:56
by: a123x
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