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Pretty Pictures (2)
Polycrystal of 5-MeO-DMT freebase :3

[file]75048[/file]

This beauty weighs about 380 mg :)

...
21-4-2019 at 05:32
by: bipolar
The Short Questions Thread (4)
Does acetonitrile react with sodium metal? If so, what are the products of this reaction?
I'm hopin ...
20-4-2019 at 23:20
by: bipolar
Improving yields of TMP methylation?
So did you took melting point of the recrystallized product? It will melt much below it's mp in the ...
20-4-2019 at 19:36
by: bipolar
Removing KOH from K-GHB
I would probably try to kill excess of KOH with citric acid, evaporate solvent from your mixture (at ...
12-4-2019 at 20:23
by: bipolar
Phenylhydrazine sulfate from the HCl salt, first attempt
[rquote=608167&tid=147664&author=DrScrabs]But K or Na anions do not disturb the reaction in ...
12-4-2019 at 06:36
by: bipolar
Phenylhydrazine sulfate from the HCl salt, first attempt
[rquote=608139&tid=147664&author=DrScrabs]Ethyl acetate does not react with phenylhydrazine ...
10-4-2019 at 11:19
by: bipolar
Phenylhydrazine sulfate from the HCl salt, first attempt
[rquote=608005&tid=147664&author=DrScrabs]Maybe I do change the extraction solven aswell, et ...
10-4-2019 at 01:10
by: bipolar
Improving yields of TMP methylation?
I meant that you will always observe solids in the reaction mixture. So you won't be able to see K2C ...
9-4-2019 at 02:36
by: bipolar
Improving yields of TMP methylation?
[rquote=607817&tid=147245&author=horribilis]and for 3 hours after all K2CO3 is dissolved[/rq ...
8-4-2019 at 12:10
by: bipolar
Improving yields of TMP methylation?
Those 'oil droplets' are probably undissolved [crude] melted 3,4,5-TMBA. This compound should have p ...
7-4-2019 at 20:43
by: bipolar
Improving yields of TMP methylation?
IMO, when doing this procedure with a solvent (DMF) you don't have to add TMP via addition funnel (j ...
7-4-2019 at 07:32
by: bipolar
Improving yields of TMP methylation?
[rquote=607298&tid=147245&author=horribilis]
Does bisulfite adduct work to purify? I unders ...
3-4-2019 at 04:17
by: bipolar
Improving yields of TMP methylation?
[rquote=607294&tid=147245&author=horribilis]Perhaps recrystallization from hexanes/heptanes ...
3-4-2019 at 03:38
by: bipolar
Myristicinaldehyde preparation (using dichloromethane)
[rquote=607289&tid=147026&author=laserlisa]Did you make the 5-hydroxyvanillin yourself?[/rqu ...
3-4-2019 at 03:01
by: bipolar
Improving yields of TMP methylation?
1. IMO, inert atmosphere is unnecessary here.

2. It is a bad idea to reflux DMF as it will decomp ...
3-4-2019 at 02:53
by: bipolar
Myristicinaldehyde preparation (using dichloromethane)
[rquote=606643&tid=147026&author=bipolar]to the reaction mixture was added CH[sub]2[/sub]Cl[ ...
3-4-2019 at 02:09
by: bipolar
Protocatecualdehyde > Piperonal ?
[rquote=607079&tid=147223&author=NewTopic]Any advice ? [/rquote]
Use conditions similar to ...
3-4-2019 at 02:01
by: bipolar
Iodine-Iodic acid 5-minute-iodination proof-test
Month ago I tested this easy iodination procedure with I[sub]2[/sub]-HIO[sub]3[/sub] system from the ...
29-3-2019 at 15:31
by: bipolar
Tryptamine is trolling?
Half a year ago I was making tryptamine by decarboxylation of tryptophan in acetophenone (at 150-180 ...
28-3-2019 at 14:44
by: bipolar
Myristicinaldehyde preparation (using dichloromethane)
I didn't find any topic dedicated to myristicinaldehyde so I started new one. Sorry if I should've U ...
27-3-2019 at 11:32
by: bipolar
5-hydroxyvanillin preparation from 5-iodovanillin
Following text below is mine very old lab records for the preparation of 5-hydroxyvanillin translate ...
26-3-2019 at 12:16
by: bipolar
Mercury-free Clemmensen reduction?
About 2 years ago I was curious whether or not non-amalgamated zinc could reduce aldehyde group. So ...
24-3-2019 at 17:03
by: bipolar

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