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diethylsulfide
Thanks everyone for their opinons, i have found an excellent alternative which should work.

My n ...
6-4-2015 at 04:16
by: chemx01
diethylsulfide
I need some diethylsulfide for my synthesis of precious metal complexes but sigma's price is too hig ...
5-4-2015 at 11:41
by: chemx01
Vanilin+K2CO3
Do you think that it is possible that vanilin could react in the following way?

Vanilin+K2CO3 --& ...
5-7-2013 at 09:16
by: chemx01
dictaphone for keeping records
Hi everyone,

i've been thinking about this one for some time and i'd like to know your opinion.
...
29-6-2013 at 00:56
by: chemx01
2,6-dimethylaniline
I'm working on a synthesis of bitrex and I need to prepare lidocaine first, for this I need 2,6-dime ...
11-5-2013 at 23:54
by: chemx01
hydrazine synthesis
That's the dilema i'm having whether add 360ml or 240ml of Ethanol. maybe rather than speculate i'm ...
10-5-2013 at 05:21
by: chemx01
hydrazine synthesis
I am currently working on a ethanolic hydrazine synthesis per instruction found at:
"Small-Scale S ...
9-5-2013 at 08:00
by: chemx01
Triboluminescent crystals
@haroldramis -
I got them from a chemical stockroom which because of REACH and similar laws had to ...
8-9-2012 at 00:33
by: chemx01
Triboluminescent crystals
Thank you for the watchglass idea I'll try that.
I used triethylamine dried by KOH and distilled fr ...
5-9-2012 at 10:22
by: chemx01
Triboluminescent crystals
Recently I got quite large amounts of europium and dysprosium oxides so I decided to prepare nitrate ...
5-9-2012 at 10:01
by: chemx01
preparation of e-caprolactone
I agree with Lambda-Eyde there is nothing like completing multistep synthesis. I already tried extra ...
6-5-2012 at 10:54
by: chemx01
preparation of e-caprolactone
I feel embarrased, I found the patent on this very same website but somehow I couldn't download it.
...
6-5-2012 at 08:42
by: chemx01
preparation of e-caprolactone
Thank you for you reply.
I tried searching for the patent in english but all I got was this:
http: ...
6-5-2012 at 07:28
by: chemx01
preparation of e-caprolactone
I want to prepare caprolactone which will be later used to make capsaicin. I found one german patent ...
6-5-2012 at 06:24
by: chemx01
Tetramethylorthosilicate synthesis
I think that the best option would be using SiCl4 and corresponding alcohol. The problem in this rea ...
3-4-2012 at 22:47
by: chemx01
Vacuum pump problem
I don't know if I understand you corectly but as I understand your boiling DCM and TEA under vacuum ...
15-3-2012 at 12:21
by: chemx01
Preparation of Styrene and Phenylacetylene from Polystyrene
I made bis(phenylethynyl)anthracene with same procedure as plastic and I got a crappy yield, but non ...
29-1-2012 at 01:33
by: chemx01
Oxalyl Chloride
Regarding the TCT method, one must think about the solvents which are used.
In the method that Saur ...
26-8-2011 at 00:13
by: chemx01
Oxalyl Chloride
I think that if you haven't used white phosphorous the equation should be 2P+5Cl2-->2PCl5 so from ...
25-8-2011 at 00:35
by: chemx01
DRY HYDROGEN CHLORIDE GAS
Are you nuts?!
Mixing conc. H2SO4 with solid NaOH, what kind of idea is that??

I remebered about ...
15-8-2011 at 08:35
by: chemx01
Tetracene and rubrene synthesis.
I'm going to prepare Rubrene as my attempt to make interesting chemioluminescent dyes and I think it ...
6-8-2011 at 10:55
by: chemx01
YouTube Science Channels
Thank you very much for kind words, i'll try to keep it up, i'll post the synthesis of Acridone toda ...
26-6-2011 at 00:35
by: chemx01
YouTube Science Channels
Hi,
I've recently upgraded my lab and bought a new camera so i'm trying to post new videos on youtu ...
25-6-2011 at 13:24
by: chemx01
Lightning rod
I'm currently upgrading my laboratory (new paint, fumehood...) and i'm wondering if it's worthwhile ...
7-6-2011 at 01:56
by: chemx01
Calcium disilicide CaSi2
I was wondering about making some CaSi2 powder to make Siloxene for luminescent reaction, but i want ...
23-4-2011 at 01:17
by: chemx01
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