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Trying for Keto-RDX
that's true, dry ice could be detrimental, the ideal reaction temp during urea additions is between ... |
21-12-2021 at 18:21
by: fredsci93 |
Quantitative NHN synthesis without Hydrazine hydrate
I didn’t test with any metal plates, I have done 3 detonations with just the cap underground and o ... |
20-12-2021 at 01:15
by: fredsci93 |
Trying for Keto-RDX
I looked a bit, I’ll probably be a very long time before I try a dry ice reaction, the smallest am ... |
19-12-2021 at 20:39
by: fredsci93 |
Quantitative NHN synthesis without Hydrazine hydrate
I haven’t extensively tested it (I did a couple detonations, 3 with one misfire where the NHN wasn ... |
19-12-2021 at 17:13
by: fredsci93 |
Quantitative NHN synthesis without Hydrazine hydrate
The NHN is lightly pressed into a PP tube and takes up ~5mm of the tube, a fuse mix is added above i ... |
19-12-2021 at 11:57
by: fredsci93 |
Trying for Keto-RDX
The main reason I haven’t tried dry ice/ethanol is because where I live the only place to get dry ... |
18-12-2021 at 12:50
by: fredsci93 |
Trying for Keto-RDX
Right, I find the hexamine addition my first time around was super difficult, but on my last run it ... |
17-12-2021 at 20:09
by: fredsci93 |
Trying for Keto-RDX
wow, that's even more intense than my runaway, after the mix spewed gas and acid all over the walls ... |
17-12-2021 at 17:29
by: fredsci93 |
Quantitative NHN synthesis without Hydrazine hydrate
I use about 200mg NHN to set off ETN, so long as the ETN is dry and medium/low density 200mg is fine ... |
17-12-2021 at 17:17
by: fredsci93 |
Quantitative NHN synthesis without Hydrazine hydrate
Yea, you’ll always lose a bit to mechanical loses, but 8g is a very nice amount, enough for 40 det ... |
17-12-2021 at 15:56
by: fredsci93 |
Trying for Keto-RDX
The reaction mix is supposed to be milky and it does tend to take up alot of volume and froth, espec ... |
17-12-2021 at 15:46
by: fredsci93 |
Trying for Keto-RDX
haha, I'm glad someone else can attest to how ridiculously exothermic the reaction is, it took me a ... |
17-12-2021 at 15:38
by: fredsci93 |
Trying for Keto-RDX
yea, that's always the bottleneck in EM, it's very hard to do det tests, oh well just have to wait f ... |
16-12-2021 at 17:32
by: fredsci93 |
Trying for Keto-RDX
For the temp, I went with 0-5C, I don’t blame you for wanting to go with a lower temp, it probably ... |
16-12-2021 at 16:25
by: fredsci93 |
Trying for Keto-RDX
HDN should be dried with an acidic/neutral desiccator like calcium nitrate/chloride, it gets sticky ... |
15-12-2021 at 13:15
by: fredsci93 |
Quantitative NHN synthesis without Hydrazine hydrate
yea, it's not an exact science, anywhere between 15% and 5% would probably work |
15-12-2021 at 00:58
by: fredsci93 |
Cleaning buchner funnel after NHN synthesis
You should probably wash it more thoroughly with hydrochloric acid if you want to use it for food pr ... |
14-12-2021 at 21:47
by: fredsci93 |
NHN synthesis not working
nice, looks like a fair bit of NHN |
14-12-2021 at 21:45
by: fredsci93 |
Quantitative NHN synthesis without Hydrazine hydrate
maybe 10-5% it doesn’t matter much, just enough to dissolve the small amount of nickel oxide |
14-12-2021 at 21:44
by: fredsci93 |
NHN synthesis not working
great stuff, the ethanol has little effect on the yield, btw what color was the NHN filtrate, if an ... |
14-12-2021 at 20:35
by: fredsci93 |
Quantitative NHN synthesis without Hydrazine hydrate
nah, it's fine just wash it with sodium hydroxide then hydrochloric acid, the hydrochloric acid clea ... |
14-12-2021 at 20:33
by: fredsci93 |
Cleaning buchner funnel after NHN synthesis
dilute sodium hydroxide wash followed by a dilute hydrochloric acid wash should work
|
14-12-2021 at 20:32
by: fredsci93 |
Hydrazine
That's good that you sorted the problem, hopefully the hydrazine freebasing will go better with the ... |
13-12-2021 at 23:46
by: fredsci93 |
NHN synthesis not working
It's safe to flush, what happened to you was the solution was too acidic so upon addition of the ble ... |
13-12-2021 at 23:44
by: fredsci93 |
First nickel nitrate synthesis... did I do it right?
First, that's a slight excess of sodium hydroxide you should use 5.9g, not that that was the problem ... |
13-12-2021 at 16:15
by: fredsci93 |
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