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Replacing RP/I with something newer.
For a short while, hyposulfinic acid was popular unto its use became known. Na2SO2 is used widely in ...
12-3-2009 at 06:44
by: haribo
Diethylamine Synthesis
Hydrolysis of diethyl formamide with NaOH.
8-3-2009 at 04:46
by: haribo
Ethyl Acetate -> Ethanol
STAB is basically insoluable with H20

What we need something that you can buy 50 Kg bags.
20-2-2009 at 08:53
by: haribo
Ethyl Acetate -> Ethanol
The problem is that to make ethanol undrinkable they add quite a lot of crap to it and since I'm mes ...
18-2-2009 at 04:16
by: haribo
Ethyl Acetate -> Ethanol
Before someone flames me for such a basic post, this has been done in an alkali (NaHCO3) enviroment ...
16-2-2009 at 09:37
by: haribo
Methods of Chlorination of Primary non Benzylic Alcohols
My god, this is getting complecated. Is there something wrong with SOCl2? It's very cheap, every sin ...
24-12-2006 at 04:58
by: haribo
3-quinuclidinol synthesis?
Some time back, the BBC made a documentry that had a lot of footage of US soldiers on various differ ...
19-12-2006 at 04:59
by: haribo
NaBH4/NiCl2 reduction
Thank god for that, I thought one of us had gone mad and I was pretty sure it was me.
19-12-2006 at 04:51
by: haribo
triethylenamine
[quote][i]Originally posted by Aqua-regia[/i]
How can I synthesise triethylenamine [/quote]

I wo ...
19-12-2006 at 04:49
by: haribo
Which extraction method to use for plants
For extracting some oils, for example safrole, steam-distillation does the trick. You can buy stills ...
17-12-2006 at 06:56
by: haribo
NaBH4/NiCl2 reduction
Errr... Could you repeat the question?
17-12-2006 at 06:50
by: haribo
NaBH4/NiCl2 reduction
I've used tbe Zinc/Nickel couple to reduce oximes and it worked very nicely. DIBAL is a bit of a pai ...
16-12-2006 at 14:26
by: haribo
Potential route to amphetamine...
If you make PEA and form an imine with methyl amine, CH3I will add to that. Someone on the Hive call ...
8-12-2006 at 11:57
by: haribo
PPA->4-MAR
Plain aminorex is 4 x stronger so I wouldn't bother.
4-12-2006 at 02:28
by: haribo
theoretical amphetamine variants
64Bandil made and tasted p-F amphetamine. He found it a slightly weaker stimulant than plain ampheta ...
3-12-2006 at 02:11
by: haribo
Amino alcohol via Akabori, trial run
That may be the case with unsubstituted varients, but it may be a useful route to substituted analog ...
2-12-2006 at 14:42
by: haribo
Amino alcohol via Akabori, trial run
Sorry about that. Yes, I'm interested in knowing if anyone has tried this particular reaction replac ...
2-12-2006 at 10:21
by: haribo
I need a new drug...
If your going for disulfiram, why not also investigate 1 amino cyclopropanol (found in some mushroom ...
1-12-2006 at 10:45
by: haribo
Amino alcohol via Akabori, trial run
Just out of interest, do you end up with a raecemic mixture? I ask because the cyanate route to 4MAR ...
29-11-2006 at 11:39
by: haribo
PPA->4-MAR
Cyanate vasoxine & add something funky to the 4 position of the phenyl ring. You now have someth ...
29-11-2006 at 11:12
by: haribo
oxime reductions
Anyone with a Hive backup should look at Labrats Zinc/Nickel couple for the reduction of oximes. It' ...
28-11-2006 at 08:38
by: haribo
PPA->4-MAR
Aminorex has been produced in 78% yield in 1 pot using 1 phenyl ethanolamine hydrochloride, HCl,KOCN ...
28-11-2006 at 08:19
by: haribo

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