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Nitrous acid production & shelf life
I made up a batch 4 months ago and it still reacts consistently. Its in a small 10 ml dropper bottle ... |
8-2-2016 at 14:05
by: hive3 |
Acetophenome Workup
What acid and base did you use in your workup? I did try a separation directly from Acetophenome usi ... |
14-1-2016 at 14:38
by: hive3 |
Acetophenome Decarb Procedure
These are my notes from an Acetophenome decarb. I am planning on dissolving the product in dry ace ... |
9-11-2015 at 12:05
by: hive3 |
It might be in calibrate mode
On one side under the unit is a leaver that drops a 100g weight internally for calibration purposes. ... |
1-9-2015 at 11:12
by: hive3 |
Report on Decarboxylation of Tryptophan in various solvents
[rquote=338168&tid=31306&author=Chemosynthesis]
Acetophenone at least used to be among the ... |
5-9-2014 at 05:42
by: hive3 |
Steam Distillation of GBL and Conversion to GBH
[rquote=331711&tid=3159&author=hive3]The extraction process is cumbersome and requires large ... |
7-7-2014 at 10:09
by: hive3 |
Distillation
The extraction process is cumbersome and requires large amounts of solvents and pulls over more impu ... |
19-5-2014 at 07:14
by: hive3 |
L-tryptophan decarboxylation
Placo,
Are you using a a sealed setup with tubing take off to blubber? There is really no way to ... |
4-2-2014 at 14:06
by: hive3 |
L-tryptophan decarboxylation
Interesting to see an attempt at that method, what extraction method did you use? Extracting is the ... |
3-1-2014 at 06:17
by: hive3 |
Sodium Borohydride from chinese supplier
I successfully purchased from this user. There was a shipping issue and it was corrected satisfactor ... |
5-12-2013 at 06:26
by: hive3 |
L-tryptophan decarboxylation
Absolutely beautiful!!!!! |
21-10-2013 at 08:38
by: hive3 |
L-tryptophan decarboxylation
I have not tried a distillation. Others who have tried using standard short path distillations seem ... |
21-10-2013 at 08:09
by: hive3 |
L-tryptophan decarboxylation
Is the 40% yield from the carbonate process? I have used the boiling heptane method and it is a time ... |
15-10-2013 at 11:54
by: hive3 |
drying with sodium metal
Purification of laboratory chemicals, D. D. Perrin has been recommended before. It can be had in an ... |
1-10-2013 at 06:30
by: hive3 |
MAOI(harmine) extraction of tobacco
In comparison to a messy Syrian rue extraction anything is preferable. The harmalas fluoresce under ... |
27-9-2013 at 05:45
by: hive3 |
MAOI(harmine) extraction of tobacco
The studies show very low levels ie 20 Billionths of a gram in the smoke. Stick with Syrian Rue. |
26-9-2013 at 12:52
by: hive3 |
L-tryptophan decarboxylation
Very nice result and an excellent yield from recrystallization. Did you record the PH before recryst ... |
4-9-2013 at 12:24
by: hive3 |
MP's
Tryptamine Melting Points
I did the MPs tonight.
MP of Filtered Tryptamine after Ammonia ... |
26-8-2013 at 17:23
by: hive3 |
Megalodon’s purification process
Thanks for the pointers. I will definitely try the boiling acidic acid extraction in the future.
... |
26-8-2013 at 04:19
by: hive3 |
Purification of Tryptamine from Crowfjord’s process
The mineral oil and participated crystals and orange oil were heated to 80C, washed 3 times with 50 ... |
25-8-2013 at 15:54
by: hive3 |
STAB
I Believe the sodiumtriacetoxyborohydride is created in situ from NaBH4 and the acidic acid. You don ... |
1-8-2013 at 13:02
by: hive3 |
Dimethylation of tryptamine via formaldehyde/STAB
[rquote=277799&tid=23682&author=turd]All tryptamine was gone on TLC (EtOAc/MeOH 2:1 with NH3 ... |
31-7-2013 at 08:01
by: hive3 |
Success with Crowfjord's mineral oil conversion
I was very excited to also see beautiful Tryptamine crystals forming from the oil 24 hours later.
... |
17-7-2013 at 11:56
by: hive3 |
Recrystalization
I have used boiling Heptane and it works very well. It requires a lot of patience though, I only see ... |
3-7-2013 at 09:29
by: hive3 |
See Also
Reductive methylation of primary and secondary amines and
amino acids by aqueous formaldehyde and z ... |
3-7-2013 at 08:52
by: hive3 |
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