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Separating Aluminum Alloy and Getting Calcium Metal Simultaneously
Making Ca is one goal. Separating 356 aluminum is another goal. My original way to do that was anhyd ... |
18-12-2021 at 08:45
by: kilowatt |
Cleaning of Alkali Metals
I need to prepare clean ampoules of cesium, and eventually rubidium and potassium for investment, us ... |
18-12-2021 at 06:10
by: kilowatt |
Cesium Reduction/Distillation
I have not gotten the material out of the retort yet. Might start that process tonight. I should kno ... |
13-12-2021 at 10:59
by: kilowatt |
Cesium Reduction/Distillation
I've seen the Codyslab video on cesium before. It's what made me think I could try this at home. I'm ... |
13-12-2021 at 09:24
by: kilowatt |
Cesium Reduction/Distillation
I have been doing this process in a small steel retort with an argon feed tube, a thermocouple well, ... |
12-12-2021 at 19:06
by: kilowatt |
Separating Aluminum Alloy and Getting Calcium Metal Simultaneously
My understanding is that heating MgCl2 hexahydrate affords MgO and HCl or something similar. Not anh ... |
7-12-2021 at 20:37
by: kilowatt |
Separating Aluminum Alloy and Getting Calcium Metal Simultaneously
Anhydrous CaCl2 is cheap and easy to buy. But anhydrous MgCl2 would require chlorination of magnesiu ... |
28-11-2021 at 13:39
by: kilowatt |
Separating Aluminum Alloy and Getting Calcium Metal Simultaneously
I'm not sure if this reaction would work, since at normal aluminum melt temperatures calcium chlorid ... |
22-11-2021 at 17:20
by: kilowatt |
Practical NOx Chemistry.
Interesting. Sounds like you came pretty close. Just need to oxygenate and distill.
I actually h ... |
18-8-2020 at 14:21
by: kilowatt |
Diethyl Ether - Keep on failing to make it -Errors
When I made ether I heated the acid up first and dripped in ethanol through an addition funnel. The ... |
17-8-2020 at 12:24
by: kilowatt |
Practical NOx Chemistry.
I produced a crude NO2/N2O4 by thermal decomposition of calcium nitrate in a stainless vessel placed ... |
17-8-2020 at 11:59
by: kilowatt |
Pretty Pictures (1)
Solid N2O4 condensing in a dewar condenser with a dry ice/ethanol bath. |
7-8-2013 at 17:54
by: kilowatt |
golfpro's Nitric Acid for Beginners
I don't believe that the acid from a simple retort is much less concentrated than if you had used a ... |
25-7-2013 at 18:51
by: kilowatt |
Onions and Syn-Propanethial-S-oxide
I have read somewhere that it doesn't, that it is a myth that it forms sulfuric acid. I do not recal ... |
24-7-2013 at 22:27
by: kilowatt |
Onions and Syn-Propanethial-S-oxide
That's exactly what I'm talking about. It should be apparent that I have already looked at that page ... |
21-7-2013 at 15:21
by: kilowatt |
Onions and Syn-Propanethial-S-oxide
I have taken somewhat of an interest in the pungent extracts of spicy/lachrymatory foodstuffs. Capsa ... |
15-7-2013 at 20:22
by: kilowatt |
Selling it all!
I would buy the DCM, glacial acetic, ethyl acetate, and sulfuryl chloride. If you have a solid form ... |
27-10-2012 at 15:45
by: kilowatt |
Copper Sulfate Production
I've been down that road of electrolysis before and found it much faster and more efficient to start ... |
24-9-2012 at 22:30
by: kilowatt |
Disagreeable Impurity in Drain Cleaner Sulfuric Acid Based Processes
Adding H2O2 to the acid would be a bit dangerous wouldn't it? If there are significant organic impu ... |
15-2-2011 at 23:01
by: kilowatt |
Disagreeable Impurity in Drain Cleaner Sulfuric Acid Based Processes
I have always used Rooto brand drain opener for synthesis processes requiring concentrated sulfuric ... |
6-2-2011 at 13:03
by: kilowatt |
Nitric + sulfuric waste
Wouldn't that just mean that the total amount of liquid goes up and up? There must be some boiling ... |
9-5-2010 at 17:36
by: kilowatt |
Nitric + sulfuric waste
Depending on the amount you could react it with excess copper oxide to get a mixed copper nitrate/su ... |
9-5-2010 at 12:20
by: kilowatt |
Nitric Acid Synthesis
[quote]
Heating NH4NO3 has to be done very carefully, as the salt is prone to unstable decompositio ... |
2-5-2010 at 23:56
by: kilowatt |
Bottles for Acids?
Are you sure they will sell to individuals? They say that they do not sell chemicals to individuals ... |
25-3-2010 at 17:09
by: kilowatt |
Bottles for Acids?
No. I have seen them on ebay for a lot less than that though! It's pretty much the only reasonable ... |
25-3-2010 at 13:09
by: kilowatt |
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