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Dioxirane amine oxidation
DMDO appears to be liable to overoxidise to the carbonyl. (find a pdf of the Wiley Encyclopedia of R ...
19-12-2022 at 04:24
by: medchemist
Grignard reaction products ?
have you tried adding a bit of HCl to see if that dissolves the Mg precipitate? You should then be a ...
23-3-2022 at 13:08
by: medchemist
Medicinal Compounds of Natural Origin
There are quite a few compounds that fit your interest. I would recommend finding a book on pharmaco ...
3-6-2021 at 14:04
by: medchemist
Pyridine hydrogenation - methods?
I searched your reaction on SciFinder, came up with one result.

Catalytic hydrogenation of subst ...
14-5-2021 at 23:44
by: medchemist
Iodination of Paracetamol
Try and react away any excess iodine, that's what the thiosulfate was used for in the original proce ...
11-3-2021 at 02:30
by: medchemist
What are most dangerous toxic chemicals you are comfortable handling in your home lab?
[rquote=653021&tid=156632&author=Fyndium]Btw, how are extremely toxic reagents like dimethyl ...
17-1-2021 at 04:07
by: medchemist
Hydrogen production for Al + Na/KOH + H2O - what is the best method for control?
What Twospoons suggested (self regulating thingy) is called a Kipp's Apparatus - You might be able t ...
27-9-2020 at 01:51
by: medchemist
Recrystallization with dual solvent system?
This is an established method, I believe it's even mentioned on the wikipedia page for recrystalliza ...
27-9-2020 at 01:47
by: medchemist
UK source for stains & microbio stuff
Hey all,
As my un suggests I'm a chemist at heart but am getting very into microbiology on a budge ...
29-6-2020 at 04:06
by: medchemist
help in selecting solvent for synthesis of phenolphthalein.
for extraction what are we trying to extract it from? i.e. what are the reagents used to make it?
12-3-2020 at 13:12
by: medchemist
UK suppliers
That's perfect! thank you very much :D
15-4-2019 at 10:07
by: medchemist
UK suppliers
Hi all,
I used to experiment at home as a teen and got most of my glassware from school and made a ...
14-4-2019 at 13:21
by: medchemist
Difficulty getting a peptide coupler.
I have a bottle HATU in the fridge at work, I'm sure a gram would go unnoticed given our scaleup wor ...
5-7-2018 at 11:37
by: medchemist
Distilling small scale Cannabis extracts
Perhaps look at vacuum distillations - by lowering the pressure you lower the boiling poi ...
12-11-2017 at 13:11
by: medchemist
Get rid of Nitrogen dioxide
let the NO2 flow over NaOH/KOH solid, it will self moisten being hydroscopic and if you have a tube ...
12-7-2015 at 14:56
by: medchemist

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