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Finally a simple method for the realitive purification of NOS
What sort of regulator connects to a big NOS tank like that? Filtering gasses sounds like a fun expe ...		 29-11-2013 at 14:57
by: megalodon
Reductive Alkylation with Thiourea Dioxide?
I know a couple posts have been about alternative pathways and thus arguably off topic, but they app ...		 16-10-2013 at 05:03
by: megalodon
Reductive Alkylation with Thiourea Dioxide?
I floated the idea of reductive amination using thiourea dioxide (thiox) a while ago in the thiox th ...		 12-10-2013 at 12:30
by: megalodon
Thiourea Dioxide --> better than borohydride?
I'd like to bring up reductive alkylation with TUD again ... has anyone had success with it?

The ...		 13-9-2013 at 10:40
by: megalodon
L-tryptophan decarboxylation
I typically get yields ~85-90% (eg, 4.5g tryptamine from 6.8 g tryptophan).

I've found that the s ...		 28-8-2013 at 15:48
by: megalodon
L-tryptophan decarboxylation
I am away from my notebook so you will have to forgive a bit of generalization and vagueness. I'll f ...		 25-8-2013 at 17:23
by: megalodon
Dimethylation of tryptamine via formaldehyde/STAB
Looking at the reaction schema for STAB given at wikipedia:

https://en.wikipedia.org/wiki/Triacet ...		 23-8-2013 at 05:54
by: megalodon
L-tryptophan decarboxylation
I would also like to thank Crowfjord for a much more pleasant decarboxylation technique :)

A bit ...		 26-7-2013 at 11:16
by: megalodon
Reductive amination without Pictet Spengler: Lilienthal's method?
[rquote=289263&tid=24700&author=Nicodem][rquote=288977&tid=24700&author=megalodon]Pe ...		 24-6-2013 at 09:08
by: megalodon
Reductive amination without Pictet Spengler: Lilienthal's method?
Perhaps I haven't made myself quite clear. I was not looking to be tutored on ring closure. I was no ...		 22-6-2013 at 05:59
by: megalodon
Reductive amination without Pictet Spengler: Lilienthal's method?
@Furboffle: Lilienthal's procedure, which I replicated, did indeed leave out an acidification step. ...		 21-6-2013 at 13:17
by: megalodon
Reductive amination without Pictet Spengler: Lilienthal's method?
That is indeed a different order. I was under the impression that Lilienthal's procedure was trying ...		 20-6-2013 at 16:28
by: megalodon
Reductive amination without Pictet Spengler: Lilienthal's method?
I have done said research, but thanks for the advice - my head is still swimming a bit in rules and ...		 20-6-2013 at 12:42
by: megalodon
Reductive amination without Pictet Spengler: Lilienthal's method?
Hi all,

I am studying organic chemistry and the basic concepts are easy to grasp (eg, substitutio ...		 19-6-2013 at 07:20
by: megalodon

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