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Isolation of primary amines as HCL salt problem
To a 40mL beaker was added 5mL n-methyl-2-beta-ethylamine-pyyrole as a brown freebase oil. This was ...
10-12-2006 at 10:41
by: mescalaniousmelvin
3,4,5-trimethoxynitrostyrene reduction fun
[quote][i]Originally posted by Biginelli[/i]
What about NaBH4 in CF3COOH for phase 1? [/quote]

S ...
26-11-2006 at 17:18
by: mescalaniousmelvin
3,4,5-trimethoxynitrostyrene reduction fun
^^^^^^^^

What do you think about scale up, what are the consequences of concenterating maybe 2-3e ...
26-11-2006 at 17:04
by: mescalaniousmelvin
3,4,5-trimethoxynitrostyrene reduction fun
It seems like LAH is not a good option as it goes kaboom, precipiates always clog the stirbar, ether ...
26-11-2006 at 12:14
by: mescalaniousmelvin

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