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2,3 dichlorobenzoyl chloride
It reacted instantly with triethylamine, producing a yellow/white solid. That seems like the expecte ...
14-7-2015 at 05:08
by: metalayer
2,3 dichlorobenzoyl chloride
I purchased some 2,3 dichlorobenzoyl chloride. This compound has an acyl chloride group but what I h ...
14-7-2015 at 03:04
by: metalayer
Fischer esterification equilibrium
Thanks for the journals. I have a clearer idea of the procedure now.

I intend to use a 3x molar e ...
12-5-2015 at 17:32
by: metalayer
Fischer esterification equilibrium
[quote]
We're not too stupid to figure out you're asking about 3',4'-Methylenedioxy-α-pyrrolidinob ...
16-4-2015 at 04:18
by: metalayer
Fischer esterification equilibrium
Is it always necessary to use a molar excess of the alcohol? The alcohol has the same solubility pro ...
16-4-2015 at 02:44
by: metalayer
Molar ratio help
Thanks, I see where I went wrong now.
28-11-2014 at 10:34
by: metalayer
Molar ratio help
Can someone check I have this right?

I need a 1.5:1 molar ratio of 6% NaOCl to 20g of an alkene w ...
28-11-2014 at 08:12
by: metalayer
Preparation of Nickel (ii) acetate
I need the solid, thanks for saving me a lot of time!
4-11-2014 at 11:49
by: metalayer
Preparation of Nickel (ii) acetate
I'm looking to make Nickel (ii) acetate from Nickel (ii) Carbonate Hexahydrate. Is it as simple as a ...
3-11-2014 at 15:19
by: metalayer
Over-oxidation of aldehyde to ketone
[rquote=352985&tid=37288&author=Crowfjord]Ah, that makes much more sense! The wording was ju ...
11-10-2014 at 09:35
by: metalayer
Oxidative C–C Bond Cleavage of Aldehydes via Visible-Light Photoredox Catalysis
http://pubs.acs.org/doi/abs/10.1021/ol303437m

May be of interest to those that stated oxidative c ...
11-10-2014 at 08:36
by: metalayer
Over-oxidation of aldehyde to ketone
[rquote=351966&tid=37288&author=Dr.Bob]You need to give some specifics for this to make any ...
8-10-2014 at 08:28
by: metalayer
Over-oxidation of aldehyde to ketone
[rquote=351833&tid=37288&author=Crowfjord]An aldehyde cannot be oxidized to a ketone. Do you ...
8-10-2014 at 05:09
by: metalayer
Over-oxidation of aldehyde to ketone
I have experimented with the over-oxidation of an aldehyde to a ketone and had some positive results ...
7-10-2014 at 20:05
by: metalayer
Arecoline extraction
[rquote=317242&tid=27854&author=DraconicAcid]Arecoline is an ester- a strong base like sodiu ...
30-1-2014 at 12:55
by: metalayer
Freebasing with NaOH
I am trying to follow a synthesis which involves making freebase Arecoline from Arecoline Hydrobromi ...
30-1-2014 at 09:24
by: metalayer
Grignard with 4-chlorophenylmagnesium bromide
Does a Grignard reaction with 4-chlorophenylmagnesium bromide require anhydrous ether? I know its po ...
16-1-2014 at 07:28
by: metalayer
Arecoline extraction
Thanks for your responses, I'm on the right track now.
10-1-2014 at 11:23
by: metalayer
Arecoline extraction
I can't find the solubility anywhere. Compound in question is Arecoline Hydrobromide.

Is there a ...
10-1-2014 at 10:35
by: metalayer
Calculating amount of solvent required
Is there a general method or equation for determining the quantity of a solvent (DCM in my case) nee ...
10-1-2014 at 09:41
by: metalayer
Grignard reagent
Does anyone have any 4-Chlorophenylmagnesium bromide (1M in ether) to sell? Or has a source better t ...
13-12-2013 at 07:53
by: metalayer
Selling reagents and glassware, cheap
bfesser is correct, those items sold. I'm a longtime lurker for what its worth :-)
8-7-2013 at 14:41
by: metalayer
Selling reagents and glassware, cheap
http://www.ebay.co.uk/sch/dcar4680/m.html?_ipg=50&_sop=12&_rdc=1

Ammonium acetate 500g
A ...
8-7-2013 at 02:58
by: metalayer

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