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1-amino-2-propanol
I would suggest propylene glycol and HaloAcetone as starting materials!

If polyols like PG follow ...
16-12-2017 at 02:47
by: mfilip62
Foundamental reactions of Organic Chemistry applien on poliols and Phenylallys?
Thanks,this is actually very interesting link but still not what I asked.

I know that diols react ...
14-12-2017 at 11:47
by: mfilip62
Foundamental reactions of Organic Chemistry applien on poliols and Phenylallys?
I was supprised to have such a hard time finding ANY usable infor or scientific papers/publications
...
14-12-2017 at 07:48
by: mfilip62
OTC synthesis of precious catalytic amines?!
I am interested if anyone knows how to make things like TMEDA and DIPEA/DIEA OTC!?

H√ľnig's base ...
14-12-2017 at 06:33
by: mfilip62
POCl3,Acyls,Anhydrides,AlkalyMetals and Halogens
Yeah,

You are right,I put too many things together...as you said! Monday!:D
And no,I don't deal ...
4-8-2017 at 01:04
by: mfilip62
POCl3,Acyls,Anhydrides,AlkalyMetals and Halogens
Greetings

I haven't beeh here a LOOONG time and I hope you guys can help me out with something th ...
29-7-2017 at 21:34
by: mfilip62
Maleic anhydride to trade
Hy,

Got 1kg of >99% Maleic anhydride pallets from Acros org. by mistake.

I ordered (and sti ...
11-11-2012 at 22:37
by: mfilip62
NaI best method?
I know about triiodide thing,that is how tinctures are made.

I think that best way is to use stoi ...
2-5-2011 at 09:34
by: mfilip62
NaI best method?
Interesting! But problem is that he adds liberal ammounts of hydroxide to unknown concetration of I2 ...
2-5-2011 at 05:28
by: mfilip62
NaI best method?
I have elementar I2.
You mean you can simply react it with NaOH!?
How!?

I got another idea,but ...
1-5-2011 at 19:00
by: mfilip62
NaI best method?
I probably did...but still,problem is that H2SO4 alone will oxydize I- to I2 and I don't have phosph ...
29-4-2011 at 11:04
by: mfilip62
NaI best method?
Thanks Mixell,

I know how this technique works in general,I done it befroe,I am just asking if so ...
29-4-2011 at 10:40
by: mfilip62
NaI best method?
Hi guys,

I am having trouble doing Finkelstein swap using KI.
NaI is best for this reaction sinc ...
29-4-2011 at 07:58
by: mfilip62
p-benzoquinone HELP!!!
Thanks on note I_Captain,very interesting to know!

No,my peroxide is 30% by mass,I got it form th ...
19-8-2010 at 11:55
by: mfilip62
p-benzoquinone HELP!!!
No need, I found this method fully documented with pictures, yield is great and pure.

I find out ...
1-8-2010 at 13:50
by: mfilip62
p-benzoquinone HELP!!!
I already did so, thanks!
Dissolved green stuff in DCM and washed it with water twice.
Green black ...
30-7-2010 at 14:54
by: mfilip62
p-benzoquinone HELP!!!
Just examined out brown-red product.
It is most probably p-benzoquinone, but very impure containing ...
29-7-2010 at 16:28
by: mfilip62
p-benzoquinone HELP!!!
I used two different sources of hydroquinone,they are fresh opened and brand new from realible compa ...
29-7-2010 at 10:17
by: mfilip62
p-benzoquinone HELP!!!
I aded more H2O2 and heated to 40,but no sucess.
You get any smelly aldehide and acid in this reac ...
29-7-2010 at 09:01
by: mfilip62
p-benzoquinone HELP!!!
That is what botthers me,it is very simple procedure but it doesn't work for me!You do it in the wat ...
29-7-2010 at 08:30
by: mfilip62
p-benzoquinone HELP!!!
Brown-red produt has m.p. of 136'C.
Yes,I need photo tutorial too see how reaction looks like in di ...
29-7-2010 at 07:05
by: mfilip62
p-benzoquinone HELP!!!
Thing that botthers me is that this stuff looks and smells completely different than pure p-benzo an ...
29-7-2010 at 05:11
by: mfilip62
p-benzoquinone HELP!!!
Yes it is me again with this stupid but unavoidable chemical.
I don't know how and why but this stu ...
28-7-2010 at 14:19
by: mfilip62
proposed reduction via Al/Ga
I had same idea ever since I sabotaged pressurized aluminum cans with chunk of Ga...

If you don't ...
20-7-2010 at 13:51
by: mfilip62
Benzoquinone from Paracetamol
Back on main subject...
I tried synthesis and it works quite well!

First time I botched it becau ...
15-7-2010 at 14:37
by: mfilip62
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