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general high-yielding one-pot procedure for the reduction of conjugated aliphatic nitro groups.
swin thinks but does not know for sure this works well for ethenes. formate salts are much better do ... |
5-2-2006 at 02:19
by: niobium |
2,5-dimethoxyphenyl-2-nitropropene synthesis - 89.3% yield
with to make 2,5-dmns it works exceptionally well, requiring usually less then 36 hours for full xta ... |
27-1-2006 at 02:59
by: niobium |
2,5-dimethoxyphenyl-2-nitropropene synthesis - 89.3% yield
Hello boys and girls,
Picking up on Stoicheomtric Steve's tradition of posting extra good procedure ... |
25-1-2006 at 12:29
by: niobium |
Aromatic Bromination w/Oxone
Zooligan,
1. KHalo/oxone halogenation on the said compound does not
work as stated on the ... |
22-1-2006 at 10:49
by: niobium |
Chlorotrimethylsilane/NaBH4 rdxn problems- HELP!
Hello.
Swin tried to reduce 35 grams of 2,5-DMNS with Chlorotrimethylsilane/NaBH4 reduction tekniq ... |
7-12-2005 at 07:33
by: niobium |
inline/parallel vacuum source
thanks hinz  swin very much appreciates ur thoughts |
22-11-2005 at 12:51
by: niobium |
inline/parallel vacuum source
Hello. Swin is in need of some advice.
Swins got 2 rotary vane vacuum pumps which pull between 21-2 ... |
22-11-2005 at 11:54
by: niobium |
2,5-dimethoxybenzaldehyde iodination
hello folks.
wanted to share for future generations to come. Swin has iodinated 2,5-dimethoxybenzal ... |
15-11-2005 at 11:01
by: niobium |
catalyst for Dimethoxybenzaldehyde->DimethoxyP2NP
Hello.
swins been trying to figure out which catalyst to use for 2,5-dimethoxyp2np synthesis...
Sw ... |
7-11-2005 at 07:55
by: niobium |
KI/Oxone oxyiodination dont work!!
Nicodem thanks for clearing that up. swins thought was the same, but needed confirmation. The fact t ... |
25-10-2005 at 06:36
by: niobium |
THANKS!
Thanks! In the meantime swin found a cheap source of AgNO3 |
20-10-2005 at 08:17
by: niobium |
KI/Oxone oxyiodination dont work!!
So can anyone suggest a decent route for iodination? either the benzaldehyde or the amine? AgNO3 is ... |
18-10-2005 at 13:04
by: niobium |
KI/Oxone oxyiodination dont work!!
Hellow fellow mad scientists...
Swin has been trying to iodinate 2 compounds : 2,5-dimethoxypheneth ... |
18-10-2005 at 06:17
by: niobium |
Perfection of the method at hand
Hello boys and girls!
This time swin was set out to prove the yields can be boosted, and the styren ... |
9-10-2005 at 11:13
by: niobium |
DMSN reduciton to hydroxyls Success
Alright. let me report something.
Swin has went on and reduced his DMNS (1 spot on tlc, purity is s ... |
7-10-2005 at 05:46
by: niobium |
Hydroxylated 2C-B/I
Hi all.
recently swin has been making some 2ci. swins using the method of varma and kabalaka using ... |
4-10-2005 at 23:31
by: niobium |
