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Electric cooling apparatus for fluid circulation
The exact way you go about modifying an appliance to make it into a chiller depends heavily on exact ...
13-6-2016 at 12:53
by: nlegaux
Electric cooling apparatus for fluid circulation
I built a chiller/recirculator for all of my condensers using an old dehumidifier. However, I think ...
9-6-2016 at 17:06
by: nlegaux
Manganese Mediated Electrochemical Oxidation of Ethanol
The density of the crude product was found to be about 0.9078g/ml. This indicates that the product, ...
8-4-2016 at 15:11
by: nlegaux
Manganese Mediated Electrochemical Oxidation of Ethanol
Recently I have been synthesizing methanoic acid for trying my hand at the eschweiler-clarke and leu ...
5-4-2016 at 17:42
by: nlegaux
Ibuprofen - Methyl ester and hydroxamic acid derivatives
Excellent work AvBaeyer! I have been wondering about Ibuprofen derivatives for a long time, and you ...
29-2-2016 at 04:46
by: nlegaux
Manganese Mediated Electrochemical Oxidation of Ethanol
I would try a higher primary alcohol, but I do not own any :(

Forming a complex of the acetaldehy ...
25-2-2016 at 17:58
by: nlegaux
Chlormequat from Choline?
Would it be possible to react a choline salt with a chlorinating agent to produce Chlormequat, simil ...
25-2-2016 at 06:12
by: nlegaux
Manganese Mediated Electrochemical Oxidation of Ethanol
Could this problem possibly be fixed by introducing an immiscible organic phase to dissolve the etha ...
24-2-2016 at 16:52
by: nlegaux
Manganese Mediated Electrochemical Oxidation of Ethanol
My graphite electrodes finally came in the mail. They seem to be working quite well; after running f ...
24-2-2016 at 15:37
by: nlegaux
Heating mantles from India
I bought a 1L unbranded Indian heating mantle from Amazon a few months back. It works well, especial ...
22-2-2016 at 11:42
by: nlegaux
Manganese Mediated Electrochemical Oxidation of Ethanol
That is quite interesting. I once attempted using MnO₂ to oxidize 4-aminophenol (from hydrolyzed P ...
19-2-2016 at 09:07
by: nlegaux
Manganese Mediated Electrochemical Oxidation of Ethanol
I'm not sure, but when I rerun it this weekend I will collect some and attempt some characterization ...
17-2-2016 at 17:37
by: nlegaux
Manganese Mediated Electrochemical Oxidation of Ethanol
Thank you for the advice blogfast! I updated the procedure with embedded photos. I will take a close ...
17-2-2016 at 17:07
by: nlegaux
Manganese Mediated Electrochemical Oxidation of Ethanol
I should be able to begin work on further characterizing the product tomorrow. As far as organizatio ...
17-2-2016 at 15:54
by: nlegaux
Manganese Mediated Electrochemical Oxidation of Ethanol

[b]1. Procedure[/b]

The electrolyte is prepared by dissolving 64g MnSO₄*H₂O, 30g (NH₄)₂ ...
17-2-2016 at 08:27
by: nlegaux
Heptane as a Grignard solvent
I recently distilled diethyl ether out of some engine starting fluid, but I now have a large amount ...
17-2-2016 at 08:10
by: nlegaux
List some BAD chemistry YouTube videos
This one is pretty sad... Skip to about 10:30.
https://www.youtube.com/watch?v=c-vUeAXjQTw

nlega ...
6-1-2016 at 18:34
by: nlegaux
Diethylamine Hydrochloride Synthesis
I was able to successfully prepare freebase diethylamine with the following procedure. I refluxed 50 ...
3-1-2016 at 15:46
by: nlegaux
Flux for zinc smelting?
Sorry if I am derailing the intended subject of this thread, but what did you do to isolate the Cd f ...
27-10-2015 at 11:05
by: nlegaux
PCB etchant
In the past I have gotten some okay results using sharpie as a mask (just in case you want to go the ...
21-10-2015 at 17:31
by: nlegaux
PID Temperature Controller
Good suggestions Sulaiman; I will cut some holes in the box to allow for better ventilation and add ...
12-10-2015 at 08:42
by: nlegaux
PID Temperature Controller
A PID temperature controller such as the one shown [url=http://imgur.com/Ltf5oxJ]here[/url] can be u ...
10-10-2015 at 10:01
by: nlegaux
Chemistry of Terephthalic acid
If it is terepthalamide, you can perform a Hofmann rearrangement to produce phenylenediamine.

nle ...
24-9-2015 at 06:15
by: nlegaux
Easy Route to Acetonedicarboxylic acid?
Would it be possible to create acetonedicarboxylic acid by reacting formaldehyde and a haloacetic ac ...
21-9-2015 at 11:16
by: nlegaux
Preparation of 2-aminophenol from Salicylic Acid
I have found hydrolysis with dilute (1M) HCl(aq) for around an hour with reflux to be a successful w ...
13-9-2015 at 12:42
by: nlegaux
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