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Is DDAC (didecyldimethylammonium chloride) a good PTC for reductions with NaBH4? Particulary I am wondering about reductions of imines in toluene/water system.	29-7-2022 at 08:05 by: phendrol
Quantitative test of a sample of ostarine Any reference to the test for fluorine?	28-4-2022 at 12:22 by: phendrol
Quantitative test of a sample of ostarine Hi! I have a sample which is suppose to be ostarine of about 99% purity. [img]https://sarmguid ...	27-4-2022 at 23:47 by: phendrol
Anhydrides from diketene instead of ketene? Can acetic anhydride be made from diketene and acetic acid?	7-4-2017 at 04:57 by: phendrol
Can Nickel Boride be prepared without NaBH4? I couldn't google out any preparation of Nickel Boride that doesn't use NaBH4. Borohydride is unavai ...	21-7-2015 at 01:17 by: phendrol
How many moles of Aluminum are needed to reduce a mole of nitromethane in a Al/Hg reduction? If you would read my whole post, you would know that I don't want to use water alone.	1-12-2014 at 07:51 by: phendrol
Can any other mercury salts be prepared from Hg2(NO3)2? The question was silly because it's obvious other salts can be prepared. But can someone share a pro ...	29-11-2014 at 01:09 by: phendrol
Can any other mercury salts be prepared from Hg2(NO3)2? Can I prepare any other salts from mercury(I) nitrate?	28-11-2014 at 17:51 by: phendrol
Oximes from nitroalkenes with FeCl2 ? Thank you for your responses.	9-11-2014 at 10:59 by: phendrol
Oximes from nitroalkenes with FeCl2 ? What would have to be the molar ratio of FeCl2 to the nitroalkene ?	9-11-2014 at 08:34 by: phendrol
Oximes from nitroalkenes with FeCl2 ? Has the possibility of reducing nitroalkenes to oximes with FeCl2 alone, crossed someones mind? D ...	8-11-2014 at 06:24 by: phendrol
Aldol condensation of protocatechualdehyde with acetone and MEK. Piperonal is not what I am interested in. Even thou it smells nice.	8-10-2014 at 01:30 by: phendrol
Aldol condensation of protocatechualdehyde with acetone and MEK. Will protocatechualdehyde condense with acetone or MEK? I couldn't find anything using the search en ...	6-10-2014 at 01:11 by: phendrol
Help! Acetone mistakenly used instead of IPA in al/hg reduction of b-nitrostyrene. I wanted to reduce about 60 grams of b-nitrostyrene in a water/acetic acid/IPA mix. 200ml/600ml/200m ...	22-8-2014 at 01:14 by: phendrol
Gradual addition of powdered KMnO4 to the reaction mixture I'm trying to figure out how to add a certain ammount of KMnO4 to the reaction mixture through about ...	10-3-2014 at 08:38 by: phendrol
Tropinone from glutardialdehyde Hi! I've got some glutardialdehyde for which I have no real use. While browsing the forum I've st ...	18-11-2013 at 04:37 by: phendrol
Catechol from salicylaldehyde I want to try the preparation of catechol from salicylaldehyde. [quote] To a solution of 122 g ...	19-10-2013 at 03:13 by: phendrol
Preparation of propionaldehyde Heating calcium formate and calcium propionate also seems easy and straightforward. Does anyone hav ...	11-9-2013 at 13:58 by: phendrol
Preparation of propionaldehyde Hey! None of the places I supply offer propionaldehyde. Does anybody have a reference to a doable ...	6-9-2013 at 00:48 by: phendrol
Oxidation of styrene to phenylacetaldehyde Well to be honest I couldn't do much because I haven't got a vacuum pump. An aspirator is no good be ...	30-1-2013 at 08:57 by: phendrol
Electrochemical oxidation of ethylbenzene to acetophenone "The electrochemical oxidation is effected in an electrochemical cell which may be a divided electri ...	29-12-2012 at 01:02 by: phendrol
Electrochemical oxidation of ethylbenzene to acetophenone I stumbled upon a pretty interesting patent lately. US 4459186, titled "Electrochemical oxidation of ...	28-12-2012 at 08:23 by: phendrol
Oxidation of styrene to phenylacetaldehyde I've managed to prepare some styrene oxide and I'm getting ready to rearrange it in the gas phase. I ...	13-12-2012 at 06:42 by: phendrol
Oxidation of styrene to phenylacetaldehyde Nicodem you are right. The extra work up is not a big problem. Most of my work will be consumed ...	30-11-2012 at 03:15 by: phendrol
Oxidation of styrene to phenylacetaldehyde The reaction is attractive because there is no problem with acquiring the reagents where I live. Fur ...	27-11-2012 at 10:31 by: phendrol
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