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Possible OTC, 'safe' methylating agents
That’s a very interesting post by Chemi Pharma on preparation of dimethyl carbonate.

Is an aut ...
27-2-2019 at 12:08
by: starlight_
Magnesium methoxide in dmso
[rquote=560661&tid=108888&author=clearly_not_atara]
starlight: was formaldehyde produced? C ...
10-12-2018 at 23:35
by: starlight_
Magnesium methoxide in dmso
[rquote=560598&tid=108888&author=morganbw]Thank you, sir, info received.
Other magnesium s ...
9-12-2018 at 15:21
by: starlight_
Magnesium methoxide in dmso
So, some results.

Magnesium methoxide was prepared from activated magnesium and anhydrous methano ...
9-12-2018 at 12:13
by: starlight_
Magnesium methoxide in dmso
[rquote=558535&tid=108888&author=unionised]Beware the reduction of dmso to dimethyl sulphide ...
3-12-2018 at 14:38
by: starlight_
Silica
Thank you both.

It appears that the hydroxlamine is removed when the post-reaction mixture is fil ...
3-12-2018 at 14:33
by: starlight_
Magnesium methoxide in dmso
[rquote=558514&tid=108888&author=clearly_not_atara]Could you just add some MeOH to DMSO foll ...
3-12-2018 at 14:25
by: starlight_
Magnesium methoxide in dmso
Magnesium methoxide can be prepared as a gel-like sludge by reacting activated magnesium metal with ...
3-12-2018 at 10:39
by: starlight_
trying to make new post
Thank you Melgar.

Your change got the post through.

I tried to make another different post tha ...
8-11-2018 at 23:51
by: starlight_
aldehyde recovery
Suitable proportions of carbonate and water to adduct can be found in here:

http://www.sciencemad ...
8-11-2018 at 08:47
by: starlight_
Tosyl sulfonhydroxamic acid
In the paper Synlett 2009, No. 13, pp 2149–2153, Tosyl sulfonhydroxamic acid is synthesised from T ...
8-11-2018 at 00:08
by: starlight_
Interesting German Nitroalkane patent
[rquote=550637&tid=102844&author=AvBaeyer]You have asked some good questions. All are easily ...
7-11-2018 at 23:49
by: starlight_
trying to make new post
Looks like it was the spam filter. Hopefully fixed by Melgar now.
7-11-2018 at 14:23
by: starlight_
Interesting German Nitroalkane patent
So we’ve all heard about the preparation of Nitroalkanes by destructive distillation of sodium alp ...
7-11-2018 at 14:21
by: starlight_
trying to make new post
I've attached the offending post as a text file

[Edited on 7-11-2018 by starlight_]
7-11-2018 at 12:57
by: starlight_
trying to make new post
Thanks j_sum, I will try again without modification of the post and we'll see if that now works.
7-11-2018 at 12:55
by: starlight_
maybe the board software thinks i'm a spammer
Just joined today and made a post with three outgoing weblinks in it.

Could that be it?
7-11-2018 at 11:50
by: starlight_
trying to make new post
Hi All,

I've tried to post a couple of times.

Post seems to show up and then disappear within ...
7-11-2018 at 10:45
by: starlight_

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