Sciencemadness Discussion Board

How to make HAuCl4.3H2O?

beerwiz - 10-11-2019 at 23:21

Every time I try to make HAuCl4.3H2O I get the red crystalline (red garnet looking) AuCl3. After all the Au is dissolved, I heat the AR solution in a sand bath at 225°C to evaporate it. The temperature must be too high and it converts to the red AuCl3 instead. Although I've tried evaporating at 100°C and it still turns to blood red AuCl3.

Any suggestions on how to get perfect and dry HAuCl4.3H2O crystals quickly?


Deathunter88 - 11-11-2019 at 08:05

Place in a sealed bag of NaOH.

beerwiz - 11-11-2019 at 18:46

How long does it take to dry up with NaOH in a sealed bag?