Sciencemadness Discussion Board

annealing of 50cm chromatography column, ideas?

Ubya - 30-4-2020 at 08:10

for my graduation my friends bought me a 50cm glass gravity chromatography column, it looks huge. I've never used it yet as i'm still making the silica gel powder for it. since i broke an addition funnel while trying to repair it, i check all my glassware for internal stress, i just look at the piece of glassware between a polarizing filter and my laptop screen showing a white background. checking this column i noticed some pretty evident stress rings

20200430_175402-1.jpg - 1.5MB 20200430_175405-1.jpg - 1.7MB 20200430_175413-1.jpg - 2.2MB

i would hate to break it while using it, so i'd like to anneal it somehow.

any ideas on how in a home envirorment?

Deathunter88 - 1-5-2020 at 01:38

You're only going to make it worse. Chromatography columns aren't heated so it will be fine.

Ubya - 1-5-2020 at 09:34

i hope that if i ever apply some positive pressure to speed the flow it doesn't crack or break