Procedure:
An isolated crucible holder was made from 2 tin cans, one 1 liter tin can, and a 620 ml tin can. The two cans were cut in half to reduce the height
and the smaller can placed into the larger can. The space between the cans was stuffed with glasswool to provide isolation. Then, four holes were
drilled 3 cm from the bottom and iron wire was then inserted through the holes in the can to provide support for the crucible. A small stainless steel
grate was then put on top of the iron wire to make a flat surface for the crucible to stand on (Photo 163). A small 75 ml porcelain crucible was put
inside the isolated crucible holder. The crucible was small enough to allow a 1.5 cm spacing from the edges, through which the exhaust gasses of the
burner can escape, and allows even heating (Photo 164). The whole assembly was put on top of a 0.8 kW butane gas burner, and 3 g potassium nitrate
added to the crucible (Photo 164,165, Note 1). The burner was lit and put on lowest setting, to prevent the porcelain crucible from cracking due to
thermal shock. Over the course of about 10 minutes, the burner flame was gradually increased. When the potassium nitrate was molten, 3 gram of copper
powder was slowly added, while stirring the melt with a thin stainless steel spatula (Photo 165,166, Note 1). Upon further heating to about 450°C,
the copper powder slowly started to become black in colour due to the formation of copper(II)oxide (Photo 167). The mixture was stirred occasionally
and strongly heated to about 520°C, as measured by an infrared thermometer. After 45 minutes of heating and stirring, the heating was gradually
lowered, upon which the potassium nitrite crystallized as long visible dendrites (Photo 168).
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