Swim ran a Al/Hg with 44g P2P and got 86% yield freebase after acid/base.
A few days later swim ran another Al/Hg with 50g P2P and got 16g freebase after
toluene extraction. Where's the other 35 or so grams? The only thing that swim did differently is use 10% NaHCO3 for the washes instead of 5%
NaOH. So where did all that oil go? Did it go out with the wash? Why?
Regards,
FF12AX7 - 16-8-2005 at 22:14
Quote:
Originally posted by FriendlyFinger
Swim ran a Al/Hg
Swim is...?Chris The Great - 16-8-2005 at 22:38
swim = Someone Who Isn't Mebio2 - 16-8-2005 at 22:58
Were the ketone and amine from the same batch?I am a fish - 17-8-2005 at 10:45
This is a chemistry forum. It is not the place for "where did my drug synthesis go wrong?" posts. Your previous drug-related posts have
been tolerated, as the topics have been relevant to chemistry as a whole. This however, is going too far.
